[NMR paper] Structure and Dynamics Perturbations in Ubiquitin Adsorbed or Entrapped in Silica Materials Are Related to Disparate Surface Chemistries Resolved by Solid-State NMR Spectroscopy
Structure and Dynamics Perturbations in Ubiquitin Adsorbed or Entrapped in Silica Materials Are Related to Disparate Surface Chemistries Resolved by Solid-State NMR Spectroscopy
Protein immobilization on material surfaces is emerging as a powerful tool in the design of devices and active materials for biomedical and pharmaceutical applications as well as for catalysis. Preservation of the protein's biological functionality is crucial to the design process and is dependent on the ability to maintain its structural and dynamical integrity while removed from the natural surroundings. The...
nmrlearner
Journal club
0
08-02-2021 05:20 PM
Dynamic Nuclear Polarization NMR as a new tool to investigate the nature of organic compounds occluded in plant silica particles #DNPNMR
From The DNP-NMR Blog:
Dynamic Nuclear Polarization NMR as a new tool to investigate the nature of organic compounds occluded in plant silica particles #DNPNMR
p.p1 {margin: 0.0px 0.0px 0.0px 36.0px; text-indent: -36.0px; font: 12.0px Helvetica}
Masion, A., et al., Dynamic Nuclear Polarization NMR as a new tool to investigate the nature of organic compounds occluded in plant silica particles. Sci Rep, 2017. 7(1): p. 3430.
https://www.ncbi.nlm.nih.gov/pubmed/28611402
nmrlearner
News from NMR blogs
0
08-07-2017 07:31 PM
[NMR paper] High-resolution Solid-state NMR Characterization of Ligand Binding to a Protein Immobilized in a Silica Matrix.
High-resolution Solid-state NMR Characterization of Ligand Binding to a Protein Immobilized in a Silica Matrix.
Related Articles High-resolution Solid-state NMR Characterization of Ligand Binding to a Protein Immobilized in a Silica Matrix.
J Phys Chem B. 2017 Aug 01;:
Authors: Cerofolini L, Giuntini S, Louka A, Ravera E, Fragai M, Luchinat C
Abstract
Solid state NMR is becoming a powerful tool to detect atomic-level structural features of biomolecules even when they are bound to - or trapped in - solid systems that lack...
nmrlearner
Journal club
0
08-02-2017 02:19 PM
Dynamic Nuclear Polarization NMR as a new tool to investigate the nature of organic compounds occluded in plant silica particles #DNPNMR
From The DNP-NMR Blog:
Dynamic Nuclear Polarization NMR as a new tool to investigate the nature of organic compounds occluded in plant silica particles #DNPNMR
p.p1 {margin: 0.0px 0.0px 0.0px 36.0px; text-indent: -36.0px; font: 12.0px Helvetica}
Masion, A., et al., Dynamic Nuclear Polarization NMR as a new tool to investigate the nature of organic compounds occluded in plant silica particles. Sci Rep, 2017. 7(1): p. 3430.
https://www.ncbi.nlm.nih.gov/pubmed/28611402
nmrlearner
News from NMR blogs
0
07-10-2017 02:13 PM
[NMR paper] (1)H-detected solid-state NMR of proteins entrapped in bioinspired silica: a new tool for biomaterials characterization.
(1)H-detected solid-state NMR of proteins entrapped in bioinspired silica: a new tool for biomaterials characterization.
http://www.bionmr.com//www.ncbi.nlm.nih.gov/corehtml/query/egifs/http:--www.nature.com-images-lo_npg.gif Related Articles (1)H-detected solid-state NMR of proteins entrapped in bioinspired silica: a new tool for biomaterials characterization.
Sci Rep. 2016;6:27851
Authors: Ravera E, Cerofolini L, Martelli T, Louka A, Fragai M, Luchinat C
Abstract
Proton-detection in solid-state NMR, enabled by high magnetic...
nmrlearner
Journal club
0
06-10-2016 10:49 PM
[NMR paper] NMR of sedimented, fibrillized, silica-entrapped and microcrystalline (metallo)proteins.
NMR of sedimented, fibrillized, silica-entrapped and microcrystalline (metallo)proteins.
http://www.bionmr.com//www.ncbi.nlm.nih.gov/corehtml/query/egifs/http:--linkinghub.elsevier.com-ihub-images-PubMedLink.gif NMR of sedimented, fibrillized, silica-entrapped and microcrystalline (metallo)proteins.
J Magn Reson. 2015 Apr;253:60-70
Authors: Ravera E, Schubeis T, Martelli T, Fragai M, Parigi G, Luchinat C
Abstract
Resolution and sensitivity in solid state NMR (SSNMR) can rival the results achieved by solution NMR, and even...
nmrlearner
Journal club
0
03-24-2015 09:58 PM
NMR of sedimented, fibrillized, silica-entrapped and microcrystalline (metallo)proteins
NMR of sedimented, fibrillized, silica-entrapped and microcrystalline (metallo)proteins
Publication date: April 2015
Source:Journal of Magnetic Resonance, Volume 253</br>
Author(s): Enrico Ravera , Tobias Schubeis , Tommaso Martelli , Marco Fragai , Giacomo Parigi , Claudio Luchinat</br>
Resolution and sensitivity in solid state NMR (SSNMR) can rival the results achieved by solution NMR, and even outperform them in the case of large systems. However, several factors affect the spectral quality in SSNMR samples, and not all systems turn out to be equally...