Young, James Robert (1982) A Study of the Adsorption of Ni(II) onto an Amorphous Silica Surface by Chemical and NMR Methods. Dissertation (Ph.D.), California Institute of Technology. http://resolver.caltech.edu/CaltechE...9062006-143724
[NMR paper] Mechanistic Insight into Nanoparticle Surface Adsorption by Solution NMR Spectroscopy in an Aqueous Gel
Mechanistic Insight into Nanoparticle Surface Adsorption by Solution NMR Spectroscopy in an Aqueous Gel
Engineering nanoparticle (NP) functions at the molecular level requires a detailed understanding of the dynamic processes occurring at the NP surface. Herein we show that a combination of dark-state exchange saturation transfer (DEST) and relaxation dispersion (RD) NMR experiments on gel-stabilized NP samples enables the accurate determination of the kinetics and thermodynamics of adsorption. We used the former approach to describe the interaction of cholic acid (CA) and phenol...
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07-17-2017 04:07 PM
[NMR paper] Mechanistic Insights into Nanoparticle Surface Adsorption by Solution NMR Spectroscopy in an Aqueous Gel
Mechanistic Insights into Nanoparticle Surface Adsorption by Solution NMR Spectroscopy in an Aqueous Gel
Engineering nanoparticle (NP) functions at molecular level requires a detailed understanding of the dynamic processes occurring at the NP surface. Here we show that the combined analysis of Dark state Exchange Saturation Transfer (DEST) and Relaxation Dispersion (RD) NMR experiments acquired on gel-stabilized samples of NP allows for accurate determination of the kinetics and thermodynamics of adsorption. We used the former approach to describe the interaction of cholic acid (CA) and...
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06-23-2017 02:24 AM
[NMR paper] Ubiquitin immobilized on mesoporous MCM41 silica surfaces - Analysis by solid-state NMR with biophysical and surface characterization.
Ubiquitin immobilized on mesoporous MCM41 silica surfaces - Analysis by solid-state NMR with biophysical and surface characterization.
Related Articles Ubiquitin immobilized on mesoporous MCM41 silica surfaces - Analysis by solid-state NMR with biophysical and surface characterization.
Biointerphases. 2017 May 31;12(2):02D414
Authors: Adiram-Filiba N, Schremer A, Ohaion E, Nadav-Tsubery M, Lublin-Tennenbaum T, Keinan-Adamsky K, Goobes G
Abstract
Deriving the conformation of adsorbed proteins is important in the assessment of...
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06-02-2017 08:33 PM
[NMR paper] How high concentrations of proteins stabilize the amorphous state of calcium orthophosphate: a solid-state NMR study of the casein case.
How high concentrations of proteins stabilize the amorphous state of calcium orthophosphate: a solid-state NMR study of the casein case.
Related Articles How high concentrations of proteins stabilize the amorphous state of calcium orthophosphate: a solid-state NMR study of the casein case.
Langmuir. 2017 Jan 17;:
Authors: De Sa Peixoto P, Silva JV, Laurent GP, Schmutz M, Thomas D, Bouchoux A, Gesan-Guiziou G
Abstract
Understanding how proteins stabilize Amorphous Calcium ortho-Phosphate (ACP) phases is of great importance in...
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01-19-2017 08:56 AM
Silica-surface reorganization during organotin grafting evidenced by 119Sn DNP SENS: a tandem reaction of gem-silanols and strained siloxane bridges
From The DNP-NMR Blog:
Silica-surface reorganization during organotin grafting evidenced by 119Sn DNP SENS: a tandem reaction of gem-silanols and strained siloxane bridges
Conley, M.P., et al., Silica-surface reorganization during organotin grafting evidenced by 119Sn DNP SENS: a tandem reaction of gem-silanols and strained siloxane bridges. Phys. Chem. Chem. Phys., 2014. 16(33): p. 17822-17827.
http://dx.doi.org/10.1039/C4CP01973C
Grafting reactive molecular complexes on dehydroxylated amorphous silica is a strategy to develop "single-site" heterogeneous catalysts. In...
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08-06-2014 08:39 PM
Nature and Structure of Aluminum Surface Sites Grafted on Silica from a Combination of High-Field Aluminum-27 Solid-State NMR Spectroscopy and First-Principles Calculations
Nature and Structure of Aluminum Surface Sites Grafted on Silica from a Combination of High-Field Aluminum-27 Solid-State NMR Spectroscopy and First-Principles Calculations
Rachel Nathaniel Kerber, Anthony Kermagoret, Emmanuel Callens, Pierre Florian, Dominique Massiot, Anne Lesage, Christophe Cope?ret, Franc?oise Delbecq, Xavier Rozanska and Philippe Sautet
http://pubs.acs.org/appl/literatum/publisher/achs/journals/content/jacsat/0/jacsat.ahead-of-print/ja3008566/aop/images/medium/ja-2012-008566_0006.gif
Journal of the American Chemical Society
DOI: 10.1021/ja3008566
...
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04-10-2012 02:44 AM
Fast Characterization of Functionalized Silica Materials by Silicon-29 Surface-Enhanced NMR Spectroscopy Using Dynamic Nuclear Polarization
Fast Characterization of Functionalized Silica Materials by Silicon-29 Surface-Enhanced NMR Spectroscopy Using Dynamic Nuclear Polarization
Moreno Lelli, David Gajan, Anne Lesage, Marc A. Caporini, Veronika Vitzthum, Pascal Mie?ville, Florent He?roguel, Fernando Rasco?n, Arthur Roussey, Chloe? Thieuleux, Malika Boualleg, Laurent Veyre, Geoffrey Bodenhausen, Christophe Cope?ret and Lyndon Emsley
http://pubs.acs.org/appl/literatum/publisher/achs/journals/content/jacsat/0/jacsat.ahead-of-print/ja110791d/aop/images/medium/ja-2010-10791d_0005.gif
Journal of the American Chemical Society...
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02-01-2011 06:33 AM
[NMR thesis] A study of the adsorption of Ni (II) onto amorphous silica surface by chemical and NM
A study of the adsorption of Ni (II) onto amorphous silica surface by chemical and NMR methods
Young, James R. (1982) A study of the adsorption of Ni (II) onto amorphous silica surface by chemical and NMR methods. Dissertation (Ph.D.), California Institute of Technology. http://resolver.caltech.edu/CaltechETD:etd-09062006-143724
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