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5/12/2011 4:08:27 AM GMT
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[Question from NMRWiki Q&A forum] demonstrative kinetics experiment
demonstrative kinetics experiment
I'm looking for a good kinetics experiment to run in the lab section of our graduate lab course. It should be a reaction that we can set up on a bench with inexpensive materials, that will take place safely in an NMR tube, and should take about one to five hours to complete at room temperature. (If done in one, then the students can witness the outcome; more than that, and they'll just set it up, watch the first few minutes of it, then leave and get the data later.) We can follow it using any high-sensitivity high-natural abundance nucleus: 1H, 19F, or...
nmrlearner
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11-21-2011 08:06 AM
[Question from NMRWiki Q&A forum] h2bc experiment
h2bc experiment
Hello nmr wikier I want to run pulprog h2bcetgpl3 on bruker instrument using adiabiatic shape pulse crp60comp.4 I determine power level sp7 in stdisp for p24 2ms on rga it is warning that d28 is negative how i adjurst this parameter.
thanks for answering in advance
with best regard feroon
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09-20-2011 05:16 PM
[Question from NMRWiki Q&A forum] h2bc experiment
h2bc experiment
Hello nmr wikierI want to run pulprog h2bcetgpl3 using adiabiatic shape pulse crp60comp.4 now how I determine power level sp7 in stdisp It is giving 90 degree rotation should I double it for 180 degree rotation for p24 2ms is enoughf or can I increase it.
thanks for answering in advance
with best regard feroon
nmrlearner
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09-13-2011 09:08 AM
[Question from NMRWiki Q&A forum] Cbcanh experiment
CBCANH EXPERIMENT
Dear NMR wikiERS
Could you please provide any reference journal or material which describe the more detailed about CBCANH experiment , its applicability , limitations and its pulse sequence to protein size
Thanking you
SRI
nmrlearner
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05-24-2011 10:00 AM
[Question from NMRWiki Q&A forum] Basics of filtered NOE experiment
Basics of filtered NOE experiment
I have not fully understood the mechanism of the filtered NOE experiment. What does it tell you? Are you able to distinguish between inter- and intradomains in a protein? How is such an experiment performed in the lab?
NMR Master student, Sweden
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nmrlearner
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03-03-2011 02:07 PM
[Question from NMRWiki Q&A forum] From what experiment only two bond correlations we can get in varian nmr?
From what experiment only two bond correlations we can get in varian nmr?
Hi., i have one compound i need only two bond correlation contours from quaternary carbon to proton. Is there any pulse sequence to find only two bond correlations ie, from quaternary carbon to protons with minimum amount of sample in "varian nmr".
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12-28-2010 05:27 AM
[NMR paper] 1H(C) and 1H(N) total NOE correlations in a single 3D NMR experiment. 15N and 13C tim
1H(C) and 1H(N) total NOE correlations in a single 3D NMR experiment. 15N and 13C time-sharing in t1 and t2 dimensions for simultaneous data acquisition.
Related Articles 1H(C) and 1H(N) total NOE correlations in a single 3D NMR experiment. 15N and 13C time-sharing in t1 and t2 dimensions for simultaneous data acquisition.
J Biomol NMR. 2003 Nov;27(3):193-203
Authors: Xia Y, Yee A, Arrowsmith CH, Gao X
Simultaneous data acquisition in time-sharing (TS) multi-dimensional NMR experiments has been shown an effective means to reduce experimental...
NMR Experiment explanation is
Linear Mode
