Why do we trun off sample spinning when we do NOESY experiment?
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Magic Angle Spinning and Oriented Sample Solid-State NMR Structural Restraints Combine for Influenza A M2 Protein Functional Insights
Magic Angle Spinning and Oriented Sample Solid-State NMR Structural Restraints Combine for Influenza A M2 Protein Functional Insights
Thach V. Can, Mukesh Sharma, Ivan Hung, Peter L. Gor’kov, William W. Brey and Timothy A. Cross
http://pubs.acs.org/appl/literatum/publisher/achs/journals/content/jacsat/0/jacsat.ahead-of-print/ja3004039/aop/images/medium/ja-2012-004039_0004.gif
Journal of the American Chemical Society
DOI: 10.1021/ja3004039
http://feeds.feedburner.com/~ff/acs/jacsat?d=yIl2AUoC8zA
http://feeds.feedburner.com/~r/acs/jacsat/~4/xappAmN-wb8
nmrlearner
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05-25-2012 07:14 PM
[Question from NMRWiki Q&A forum] spinning heating sample in MAS
spinning heating sample in MAS
there are two known mechanisms: friction heating( which may cause several degrees temperature increase) and induced AC current heating( in this paper:Electrical and ionic conductivity effects on magic-angle spinning nuclear magnetic resonance parameters of CuI. which can heat sample over 100 Celsius.)My question is, has any body seen this heating in MAS NMR?
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nmrlearner
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04-30-2012 05:23 AM
[Question from NMRWiki Q&A forum] 2DNOESY with N15 C13 Labelled sample or Unlabelled sample
2DNOESY with N15 C13 Labelled sample or Unlabelled sample
Dear Friends, I am in process of doing structure calculation of dimeric protein 22kD by using ARIA2.2 . Can I acquire 2DNOESY spectrum for my protein. Will it provide useful information for structure calculation? And whether I should acquire 2DNOESY with N15 C13 Labelled sample or Unlabelled sample . Which sample would be appropriate for this kind of experiment on VNMRJ 700 with biopack ?
Thanks & Regards Srinivas
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nmrlearner
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02-06-2012 03:54 PM
[NMRpipe Yahoo group] Re: A sample 4D HCCH Noesy spectrum
Re: A sample 4D HCCH Noesy spectrum
This is an example for an HN-Methyl 4D I have, not exactly the same, but perhaps useful to see anyway ... the processing scheme is a very basic one ...
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12-13-2011 02:46 AM
[NMRpipe Yahoo group] Re: A sample 4D HCCH Noesy spectrum
Re: A sample 4D HCCH Noesy spectrum
Hi Have you tried the example from NMRDraw macro editor? (under process 4D) I believe nothing is special in term of processing data. Phasing, sweep width, and
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12-10-2011 02:38 AM
[NMRpipe Yahoo group] A sample 4D HCCH Noesy spectrum
A sample 4D HCCH Noesy spectrum
Hello, I'm struggling to process a 4D methyl noesy spectrum collected on a Bruker and I was wondering if anyone knows where I could find an example ser file
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12-10-2011 02:38 AM
[NMR paper] The 3D NOESY-[(1)H,(15)N,(1)H]-ZQ-TROSY NMR experiment with diagonal peak suppression
The 3D NOESY--ZQ-TROSY NMR experiment with diagonal peak suppression.
Related Articles The 3D NOESY--ZQ-TROSY NMR experiment with diagonal peak suppression.
Proc Natl Acad Sci U S A. 1999 Aug 17;96(17):9607-12
Authors: Pervushin KV, Wider G, Riek R, Wüthrich K
In our 3D NOESY--ZQ-TROSY experiment, the TROSY principle (transverse relaxation-optimized spectroscopy) is used in three-dimensional (3D) (15)N-resolved nuclear Overhauser enhancement spectroscopy (NOESY), which enables resonance assignments by sequential nuclear Overhauser effects and...
nmrlearner
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11-18-2010 08:31 PM
[NMR paper] Proton NMR studies of a large protein. pH, substrate titrations, and NOESY experiment
Proton NMR studies of a large protein. pH, substrate titrations, and NOESY experiments with perdeuterated yeast phosphoglycerate kinase containing histidine residues.
Related Articles Proton NMR studies of a large protein. pH, substrate titrations, and NOESY experiments with perdeuterated yeast phosphoglycerate kinase containing histidine residues.
J Magn Reson B. 1994 Oct;105(2):157-66
Authors: Pappu KM, Serpersu EH
Fully deuterated yeast phosphoglycerate kinase (PGK) was prepared biosynthetically with only histidine side chains of normal...