Question from NMRWiki Q&A forum spinning heating sample in MAS

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[Question from NMRWiki Q&A forum] spinning heating sample in MAS

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Fragment-based:

Rosetta-NMR (Robetta)

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GeNMR

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Torsion angles from chemical shifts:

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Promega- Proline

Secondary structure from chemical shifts:

CSI (via RCI server)

TALOS

MICS caps, β-turns

d2D

PECAN

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RCI

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HADDOCK

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Methyl S2

B-factor

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CH3shift- Methyl

ArShift- Aromatic

ShiftS

Proshift

PPM

CheShift-2- Cα

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Shifty

Camcoil

Poulsen_rc_CS

Disordered proteins:

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CCPN

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Solid-state NMR:

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04-30-2012, 05:23 AM

nmrlearner

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spinning heating sample in MAS

spinning heating sample in MAS

there are two known mechanisms: friction heating( which may cause several degrees temperature increase) and induced AC current heating( in this paper:Electrical and ionic conductivity effects on magic-angle spinning nuclear magnetic resonance parameters of CuI. which can heat sample over 100 Celsius.)My question is, has any body seen this heating in MAS NMR?

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