Question from NMRWiki Q&A forum spin lock 1H spectrum

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[Question from NMRWiki Q&A forum] spin lock 1H spectrum

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Structure from NMR restraints:

Ab initio:

Fragment-based:

Rosetta-NMR (Robetta)

Template-based:

GeNMR

I-TASSER

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Amber

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Fragment-based:

Homology-based:

Torsion angles from chemical shifts:

Preditor

TALOS

Promega- Proline

Secondary structure from chemical shifts:

CSI (via RCI server)

TALOS

MICS caps, β-turns

d2D

PECAN

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RCI

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HADDOCK

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SAVES2 or SAVES4

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Backbone S2

Methyl S2

B-factor

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Shiftx2

Sparta+

Camshift

CH3shift- Methyl

ArShift- Aromatic

ShiftS

Proshift

PPM

CheShift-2- Cα

From sequence:

Shifty

Camcoil

Poulsen_rc_CS

Disordered proteins:

MAXOCC

Format conversion & validation:

CCPN

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NMR sample preparation:

Protein disorder:

DisMeta

Protein solubility:

Isotope labeling:

Solid-state NMR:

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01-08-2014, 11:23 AM

nmrlearner

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spin lock 1H spectrum

spin lock 1H spectrum

Please, if somebody wants to help me?! I need to get 1H spectrum with spin lock pulse on Bruker AV 600 instrument. Which pulse sequence and which parameters should be used, please? Thank you, thank you, Marijana from Croatia

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