HII am faceing spining problem on av-300 bruker instrument.I have change spinner,clean shim stack but the problem is still there have any body idea what i have do now,I have check by turning on and off spinner change spin rate but it not getting spinning.IS it electronic fault?
with regardferoon
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[Question from NMRWiki Q&A forum] 2DNOESY with N15 C13 Labelled sample or Unlabelled sample
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Dear Friends, I am in process of doing structure calculation of dimeric protein 22kD by using ARIA2.2 . Can I acquire 2DNOESY spectrum for my protein. Will it provide useful information for structure calculation? And whether I should acquire 2DNOESY with N15 C13 Labelled sample or Unlabelled sample . Which sample would be appropriate for this kind of experiment on VNMRJ 700 with biopack ?
Thanks & Regards Srinivas
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http://www.nmr2.buffalo.edu/nesg.wiki/NMR_Sample_Preparation
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<!-- start content --> <table style="width: 76px; height: 63px;" id="toc" class="toc" summary="Contents"><tbody><tr><td>Contents
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08-16-2010 04:04 AM
Sample preparation
Sample preparation Samples
The Samples program is designed to collect and store some essential information pertaining to the samples used to record the spectra.
Residual Dipolar Couplings
Bicelle preparation notes from Avanti
Instructions for bicelle preparation from Avanti