Hi, everybody! I met a problem on Varian 400 MR: DMSO samples don't lock by "find Z0" button, but I can find lock signal manually in a quite unusual range of Z0 values (30000). After adjusting shims i still have pour s/n. Probe is tuned and matched. It happened after VT experiments, I ran. Samples in CDCl3 looks perfect! What am I doing wrong and why that's happened? Thanks.
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