Hello all, I am experiencing a problem similar to one posted about in June 2008 (message ID: 1752), only the solutions given then aren't working for me.
[NMRpipe Yahoo group] Re: Issues processing 2D SoFast HMQC
Re: Issues processing 2D SoFast HMQC
Hi Nichole, Iam extremely sorry about the previous post. if you have mistakenly used nd0=2 for sfhmqc, try changing this line in the nmrPipe script from -xSW
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09-05-2012 03:35 AM
[NMRpipe Yahoo group] Re: Issues processing 2D SoFast HMQC
Re: Issues processing 2D SoFast HMQC
Hi Nicole, Pls check your sfhmqc experimental parameter 'nd0' ( using the command 'ased'). For sfhmqc the nd0 should be 1( for conventional HSQC nd0=2 ). If
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09-05-2012 03:35 AM
[NMRpipe Yahoo group] Re: Issues processing 2D SoFast HMQC
Re: Issues processing 2D SoFast HMQC
Hi Jana, I'm sorry, I should have been more clear in my post. I do use States-TPPI when processing the SoFast data. (I have also tried a plethora of other
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09-05-2012 03:35 AM
[NMRpipe Yahoo group] Re: Issues processing 2D SoFast HMQC
Re: Issues processing 2D SoFast HMQC
Hi Nicole, The yMode is not Echo-AntiEcho for the ppg sfhmqcf3gpph, it should be -yMODE States-TPPI Pls check the first line:- -bad 0.0 -noaswap -DMX -decim
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09-05-2012 03:35 AM
[Question from NMRWiki Q&A forum] 1H-119Sn HMBC or HMQC
1H-119Sn HMBC or HMQC
Dear experts,I want to run 1H-119Sn HMBC or HMQC, but I don't know the name of pulse program in Bruker.Do you know the name and any details regarding these measurements?Warmly thanks,
Check if somebody has answered this question on NMRWiki QA forum
nmrlearner
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06-24-2012 03:21 PM
[NMRpipe Yahoo group] 3d c13 hmqc noesy
3D C13 HMQC NOESY
Hello! I am looking for a script model for 3D C13 HMQC NOESY processing. It's my first 3D experiment and I need a starting point. Thanks in advance.
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02-27-2012 06:56 AM
[U. of Ottawa NMR Facility Blog] 19f - 13c hmqc
19F - 13C HMQC
If one has an NMR spectrometer with hardware capable of synthesizing and amplifying the frequency of 19F from the 1H channel and a broadband NMR probe whose 1H channel can tune down to 19F, then one is able to do 19F - 13C HMQC experiments. The figure below shows an example of a 19F - 13C HMQC spectrum collected on a Bruker AVANCE 500 NMR spectrometer using a 5 mm broadband probe. The fluorine spectrum is plotted on the top and the 13C spectrum is plotted on the side. The panel on the left shows the spectrum optimized for one-bond coupling, while that on the right shows the...
nmrlearner
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08-21-2010 08:15 PM
15N SOFAST-HMQC to study fast H-D exchange
Very Fast Two-Dimensional NMR Spectroscopy for Real-Time Investigation of Dynamic Events in Proteins on the Time Scale of Seconds
Paul Schanda and Bernhard Brutscher
J. Am. Chem. Soc.; 2005; 127(22) pp 8014 - 8015
http://pubs.acs.org/isubscribe/journals/jacsat/127/i22/figures/ja051306en00001.gif
Abstract:
We demonstrate for different protein samples that 2D 1H-15N correlation NMR spectra can be recorded in a few seconds of acquisition time using a new band-selective optimized flip-angle short-transient heteronuclear multiple quantum coherence experiment. This has enabled us to...