Is it possible to obtain this experiment with a BBI 400 MHz probe? All the tries I have made they have been unsuccessful
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[Question from NMRWiki Q&A forum] Calibration of a Bruker NMR probe
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http://www.process-nmr.com/TD-NMR1.gif
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5/12/2011 4:08:27 AM GMT
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[Question from NMRWiki Q&A forum] Tuning probe failed after a dual probe was replaced with a BBI probe
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We generally use Dual to run 13C and BBI to run 2D. After changed the probe, the command "edhead" was used to set the probe. Put the sample tube, lock the solvent, and then type "atma" to tune the probe. We always do it like this, but now we can not tune the proton after installed the BBI probe (13C is OK). The dip can not be found by "atma", and "atmm" was also not work on forming a dip. What is the most possible reason for this error? How to solve it and avoid it in the future ? Thanks. (Instrument: Bruker 400 MHz,...
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Related Articles Solid-state dipolar INADEQUATE NMR spectroscopy with a large double-quantum spectral width.
J Magn Reson. 1999 Jan;136(1):86-91
Authors: Hong M
A technique for obtaining dipolar-mediated INADEQUATE NMR spectra with a large spectral window in the double-quantum dimension is presented. Using the dipolar recoupling sequence C7 to excite the double-quantum coherence under magic-angle spinning, the technique involves incrementing the...
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