Question from NMRWiki Q&A forum How to set up an instrument for 11B NMR?

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[Question from NMRWiki Q&A forum] How to set up an instrument for 11B NMR?

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07-16-2012, 06:33 PM

nmrlearner

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How to set up an instrument for 11B NMR?

How to set up an instrument for 11B NMR?

Ok, on this particular Agilent MR400 we have a OneProbe with a ProTune module. It's presently set up and calibrated for 1H, 13C, 15N, F, and P. I would like to add 11B to the list. But we're currently lacking spectroscopist who could show me how to do it in the department.

I imagine there are 3 steps... Setup up ProTune for 11B, the calibrate the probe for 11B, and finally set up experiments for 11B. Unfortunately I don't really know how to do much on any of this and it's certainly not in the manual.

Where might I find resources for this?

Thanks,

Ken

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