I run a 1H-15N HMBC experiment on a Bruker AVANCE III 600 MHz spectrometer. But I fail to get the long- range correlation signal. please help me to set the acquisition parameters of the 1H-15 HMBC experiment, especially the “cnst2” (J(XH)) and the “cnst13” (J(XH) long range), or other key parameters.
Thank you very much!
Check if somebody has answered this question on NMRWiki QA forum
Did you find this post helpful? |
Similar Threads
Thread
Thread Starter
Forum
Replies
Last Post
[NMRpipe Yahoo group] Re: processing hmbc
Re: processing hmbc
Dear Andrew, Thank you for answer. I talked to our facility manager and he said that he usually uses phase sensitive detection for HMBC for example
More...
NMRpipe Yahoo group news
News from other NMR forums
0
11-11-2011 08:26 AM
[NMRpipe Yahoo group] Re: processing hmbc
Re: processing hmbc
Anna Kuznetsova asks about processing an HMBC. I think the key quote is "So instead of many absorptive peaks of HMBC I get 4 times more peaks with alternating
More...
NMRpipe Yahoo group news
News from other NMR forums
0
11-09-2011 06:44 AM
[NMRpipe Yahoo group] Re: processing hmbc
Re: processing hmbc
Thanks for this thorough and helpful response from Andrew. Just to amplify one item ... the nmrPipe "FT" function will work with any number of points. It will
More...
NMRpipe Yahoo group news
News from other NMR forums
0
11-09-2011 06:44 AM
[NMRpipe Yahoo group] Re: processing hmbc
Re: processing hmbc
Hi Anna, Typically, the HMBC acquisition is absolute value mode, so -yMODE and -aq2D should be "Real" and "Magnitude", respectively, and -yT and -yN should be
More...
NMRpipe Yahoo group news
News from other NMR forums
0
11-09-2011 06:44 AM
[NMRpipe Yahoo group] Re: processing hmbc
Re: processing hmbc
Dear Eugene, Thank you for answer! Actually I have figured out how to process HMBC with nmrpipe. It turned out pulse sequence I was using for HMBC is phase
More...
NMRpipe Yahoo group news
News from other NMR forums
0
11-09-2011 06:44 AM
[NMRpipe Yahoo group] Re: processing hmbc
Re: processing hmbc
Dear Andrew, Thank you for answer. I talked to our facility manager and he said that he usually uses phase sensitive detection for HMBC for example
More...
NMRpipe Yahoo group news
News from other NMR forums
0
11-09-2011 06:44 AM
[NMRpipe Yahoo group] processing hmbc
processing hmbc
Hi everybody, I am processing HMBC experiment with nmrPipe and I am using standard scripts below. In first script since I have xN 478 data points I made xT
More...
NMRpipe Yahoo group news
News from other NMR forums
0
11-09-2011 06:44 AM
[NMRpipe Yahoo group] Re: processing hmbc
Re: processing hmbc
Thank you, Andrew, very much!! I will try this. I am using hmbcetgpnd from Bruker, which is almost the same as I guess. Thank you for very helpful comments
More...