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Old 02-23-2012, 09:08 PM
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Default High Pressure NMR Samples

High Pressure NMR Samples

I need to run NMR on samples of anhydrous ammonia. The boiling point of anhydrous ammonia is -33.34 deg C. In order to be able to have enough time to acquire spectra, I would like to seal the NMR tubes. Once the sample tubes are sealed, the ammonia will build up pressure until it reaches equilibrium and exists as a liquid at room temperature (at approximately 10 atm of pressure). I know NMR tubes exist which can easily withstand these sorts of pressures, but my main problem is in finding a way to seal the tube. I have tried sealing the tubes by melting the glass, but the heating renders the glass weakened and unable to withstand the pressure. How might I be able to seal these samples effectively? Thanks for any help.



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