Hello, could you tell me which HSQC and E-HSQC program are recommendable ?
These are Bruker HSQC pulse programs:
hsqcph, hsqcphpr, hsqcphps, hsqcgpph. hsqcgpph2. hsqcetgp. hsqcetgpsp. hsqcetgpsp.2. hsqcetgpsp.3, hsqcetgpsi. hsqcetgpsi2. hsqcetgpsisp. hsqcetgpsisp2. hsqcetgpsisp.2. hsqcetgpsisp2.2, hsqcdhetgpsp, and so on.
There are Bruker E-HSQC pulse programs:
hsqcedgpph, hsqcedetgp, hsqcedetgpsp, hsqcedetgpsp.3, hsqcedetgpsisp, hsqcedetgpsisp.2, hsqcedetgpsisp2, hsqcedetgpsisp2.2, hsqcedetgpsisp2.3, and so on.
I have a few mg of my sample to be determined but it probably has one insensitve carbon on 1D-13C experiments. I would like to find and assign this carbon with HSQC or E-HSQC.
Thanks.
Check if somebody has answered this question on NMRWiki QA forum
Did you find this post helpful? |
Similar Threads
Thread
Thread Starter
Forum
Replies
Last Post
1H-15N HSQC, edited by a 1H inversion recovery and observed in the antiphase component (IR-HSQC-AP)
Could someone explain the experimental theory/basis behind 1H-15N inversion recovery filtered HSQC experiment observed in antiphase (IR-HSQC-AP)? I am still learning basic NMR theory, but would like to know about this particular experiment, which was used to detect paramagnetically broadened backbone resonances. Thanks.
Abstract
Biogenesis of iron–sulfur cluster proteins is a highly regulated process that requires complex protein machineries. In the cytosolic iron–sulfur protein assembly machinery, two human key proteins—NADPH-dependent diflavin oxidoreductase 1 (Ndor1) and...
talderson
NMR Questions and Answers
0
09-23-2013 06:01 AM
[NMRpipe Yahoo group] Re: Phasing 1H-15N HSQC Kinetics data from Bruker Instrument
Re: Phasing 1H-15N HSQC Kinetics data from Bruker Instrument
De. DeRose, Thank you for directing me to the "macro edit" pull down in NMRDraw. This, in addition to your comment regarding dwell times, has seemed to solve
More...
NMRpipe Yahoo group news
News from other NMR forums
0
08-10-2011 02:15 AM
[NMRpipe Yahoo group] Re: Phasing 1H-15N HSQC Kinetics data from Bruker Instrument
Re: Phasing 1H-15N HSQC Kinetics data from Bruker Instrument
Hi Nicole, If the first data point in the indirect dimension started at half the dwell time, the phase correction in the indirect dimension should be -p0 -90
More...
NMRpipe Yahoo group news
News from other NMR forums
0
08-06-2011 01:27 AM
[NMRpipe Yahoo group] Phasing 1H-15N HSQC Kinetics data from Bruker Instrument
Phasing 1H-15N HSQC Kinetics data from Bruker Instrument
Hello group! I should mention that my lab specializes in X-Ray Crystallography and my thesis project has me learning NMR. So, I apologize for the perhaps
More...
NMRpipe Yahoo group news
News from other NMR forums
0
08-05-2011 01:25 AM
[Question from NMRWiki Q&A forum] Looking for hsqc-based ZZ exchange bruker pulse program
Looking for hsqc-based ZZ exchange bruker pulse program
hi nmrwikier !
Anyone know if the hsqc-based zz exchange pulse prog developed by Farrow et al. (1994) is available on standart bruker pulse prog library and what is its name ?
Many thanks !
nmrlearner
News from other NMR forums
0
07-06-2011 06:14 AM
[Question from NMRWiki Q&A forum] Which Bruker HMBC program do you use?
Which Bruker HMBC program do you use?
Hello,
Here are Bruker hmbc pulse programs (produced by ls *hmbc*):
hmbcacbigpl2ndqf hmbcacgplpqf hmbcetgpl2nd hmbcgplpndqf hmbclpndqf hmbcndpsqf hmbcacgplpndqf hmbcetgpjcl2nd hmbcgpl2ndqf hmbcgpndqf hmbcndprqf shmbcgpndqfWhich would you run and for what reason?
(... I know that hmbcetgpjcl2nd - is a J-HMBC for measuring J coupling constants - what about the others?)