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[Question from NMRWiki Q&A forum] bigger MAS-NMR spectrum as irradiation window

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12-17-2014, 08:03 AM

nmrlearner

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bigger MAS-NMR spectrum as irradiation window

bigger MAS-NMR spectrum as irradiation window

Hi,

I have a sample with a very very big CSA which is broader than my irradiation windows, so I have to acquire my data in 2 or more experiments (shaped pulses are enough and I can't go for another probehead). I need to do a simulation of the resulting spectrum, but I have to make sure my irradiation power is the same everywhere so the resulting sum spectrum isn't distorted. I heard about an article about how to choose the different irradiation windows of each measure so the sum still can be simulated but I couldn't get the source. I can't find it. Has anyone ever heard of it ? Can someone give me the reference? Thanks for your help

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