This may be a daft question, but how do I go about identifying the probe in our NMR machine, and hence whether it's capable of measuring (simple 1D) 19F spectra? It is a Bruker Avance 500, and I was under the impression that it might be capable of this with a little fiddling (http://www.chem.uic.edu/nmr/download...Guide.0201.pdf), if I'm lucky wrt to what probe we have.
Thanks
Addition (1724, 260911): I have now confirmed that it is a BBO probe. What else is needed for the linked protocol to work (specific preamplifiers?), and is there a software method to check whether we have it?
(Background: our NMR tech seemed to suggest that it's not possible, but has also in the past said that VT and DOESY were not possible, and thanks to people working it out, they are now standardish here. I won't necessarily have a problem, but want to ener the conversation armed with the info, references/instructions)
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[Question from NMRWiki Q&A forum] Tuning probe failed after a dual probe was replaced with a BBI probe
Tuning probe failed after a dual probe was replaced with a BBI probe
We generally use Dual to run 13C and BBI to run 2D. After changed the probe, the command "edhead" was used to set the probe. Put the sample tube, lock the solvent, and then type "atma" to tune the probe. We always do it like this, but now we can not tune the proton after installed the BBI probe (13C is OK). The dip can not be found by "atma", and "atmm" was also not work on forming a dip. What is the most possible reason for this error? How to solve it and avoid it in the future ? Thanks. (Instrument: Bruker 400 MHz,...
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Paperback. From the initial observation of proton magnetic resonance in water and in paraffin, the discipline of nuclear magnetic resonance has seen unparalleled growth as an analytical method. Modern NMR spectroscopy is a highly developed, yet still evolving, subject which finds application in chemistry, biology, medicine, materials science and geology. In this book, emphasis is on the more...