Question from NMRWiki Q&A forum 19F full range homodecoupling

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[Question from NMRWiki Q&A forum] 19F full range homodecoupling

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NMR processing:

MDD

NMR assignment:

Backbone:

Side-chains:

NOEs:

Structure from NMR restraints:

Ab initio:

Fragment-based:

Rosetta-NMR (Robetta)

Template-based:

GeNMR

I-TASSER

Refinement:

Amber

Structure from chemical shifts:

Fragment-based:

Homology-based:

Torsion angles from chemical shifts:

Preditor

TALOS

Promega- Proline

Secondary structure from chemical shifts:

CSI (via RCI server)

TALOS

MICS caps, β-turns

d2D

PECAN

Flexibility from chemical shifts:

RCI

Interactions from chemical shifts:

HADDOCK

Chemical shifts re-referencing:

NMR model quality:

NOEs, other restraints:

Chemical shifts:

RDCs:

Pseudocontact shifts:

Protein geomtery:

SAVES2 or SAVES4

Quality Control Check

NMR spectrum prediction:

FANDAS

MestReS

V-NMR

Flexibility from structure:

Backbone S2

Methyl S2

B-factor

Molecular dynamics:

Gromacs

Amber

Antechamber

Chemical shifts prediction:

From structure:

Shiftx2

Sparta+

Camshift

CH3shift- Methyl

ArShift- Aromatic

ShiftS

Proshift

PPM

CheShift-2- Cα

From sequence:

Shifty

Camcoil

Poulsen_rc_CS

Disordered proteins:

MAXOCC

Format conversion & validation:

CCPN

From NMR-STAR 3.1

Validate NMR-STAR 3.1

NMR sample preparation:

Protein disorder:

DisMeta

Protein solubility:

Isotope labeling:

Solid-state NMR:

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06-02-2014, 10:02 PM

nmrlearner

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19F full range homodecoupling

19F full range homodecoupling

Greetings,this is my first question in this wiki :)

I wonder if there's possibility to obtain full homo decoupled spectrum of 19F. Spectrum of my compound is quite complicated becouse of 19F-19F couplings. I have BBOF probe for Bruker Avance III HD spectrometer. 19F is tuned at broadband coil. If there's any possibility to make that, please give me some clues.Thanks,Arek

EDITI have obtained projection that looks like the one I need. Projection from 2D 19F J-res spectrum. I wonder if there's some kind of pureshift experiments designated for fluorine

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