Hi Pipers, I am probably talking about a very simple issue. I want to process a 13C (detected) -15N correlation in the solid state. The spectrum was recorded
[Question from NMRWiki Q&A forum] 1h detected 3d in solids
1h detected 3d in solids
I am trying to set up a 3d 1h detected exp in solid.working on 700 MHz spectrometer,with a 3.2 mm probe.normal zg on 13c, is good ( so sample is fine).the problem occurs that i have two cp( cross polarisation) transfers steps in my 3d exp, I am not able to get 1D 1H signal out of 3d exp.the exp with the cp works well on 600 MHz spectrometer though.is it a probe problem or a magnetic field inhomogeneity?any clue will be appreciated.
Check if somebody has answered this question on NMRWiki QA forum
[NMRpipe Yahoo group] Re: Baseline issues in directly detected proton dimension of 13C-HSQ
Re: Baseline issues in directly detected proton dimension of 13C-HSQ
Hi Justin, This sensitivity enhanced experiment usually achieves good water suppression, but you could try removing some of the water with a polynomial solvent
More...
[NMR analysis blog] Mnova 6.0, at last! GSD, Line Fitting, Data Analysis, handling of LC/GC/MS data and m
Mnova 6.0, at last! GSD, Line Fitting, Data Analysis, handling of LC/GC/MS data and much more!
It's been over 6 weeks since my last post on this blog but don’t worry, I haven’t been idle. On the contrary, I have a very good excuse for this lack of posts: We all at Mestrelab have been working very hard trying to get version 6.0 of Mnova finished. Now I’m delighted to announce that we have done it and version 6.0 is finally available for download from our Web site. This is certainly a major upgrade of the software in which we have put a lot of work and passion. It brings a number of...