[Stan NMR blog] Keep your spinners smooth and clean!
Keep your spinners smooth and clean!
Illustration of artifacts caused by a dirty spinner
Source: Stan blog library
nmrlearner
News from NMR blogs
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01-30-2011 05:52 AM
Clean STD-NMR spectrum for improved detection of ligand-protein interactions at low c
Clean STD-NMR spectrum for improved detection of ligand-protein interactions at low concentration of protein.
Related Articles Clean STD-NMR spectrum for improved detection of ligand-protein interactions at low concentration of protein.
Magn Reson Chem. 2010 Oct 18;
Authors: Xia Y, Zhu Q, Jun KY, Wang J, Gao X
Saturation transfer difference (STD)-NMR has been widely used to screen ligand compound libraries for their binding activities to proteins and to determine the binding epitopes of the ligands. We report herein, a Clean STD-NMR method...
nmrlearner
Journal club
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10-22-2010 06:02 AM
[U. of Ottawa NMR Facility Blog] Retrieving Empty Spinners From Magnets
Retrieving Empty Spinners From Magnets
Despite my best efforts in teaching students how to properly use NMR spectrometers, invariably a new user will, on occasion, drop a sample spinner into a magnet without a sample. This is usually done in our undergraduate laboratory by inexperienced students who have finished collecting their data and feel a need to return the empty spinner to the magnet. The problem is that ejecting the empty spinner with the eject air is not possible as the air passes through the spinner. In the past I have removed empty rotors from magnets on Varian spectrometers by...
nmrlearner
News from NMR blogs
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08-21-2010 08:15 PM
Easy way to clean NMR tube
Easy way to clean NMR tube
This article demonstrate the easy way to clean NMR tubes. It's simple but quite useful for those working with NMR.
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