If you've ever built your own RF circuit for NMR you know that calculating the inductance for a solenoid can be challenging. This article gives some insight where the discrepancies are coming from and how to make the prediction more accurately. However, in the end you still need to get the soldering iron out and adjust capacitors to make it work.
Giovannetti, Giulio, and Francesca Frijia. “Inductance Calculation in Magnetic Resonance Solenoid Coils with Strip and Wire Conductors.” Applied Magnetic Resonance 51, no. 8 (August 2020): 703–10.
Solenoids are employed in Magnetic Resonance (MR) as radiofrequency (RF) coils due to their high sensitivity. In particular, their cylindrical symmetry is optimal for circular cross-sectional samples. Solenoid inductance estimation is a constraint for a correct design and tuning of the resonant circuit constituting the RF coil, suitable to be used for transmitting and receiving the RF signal of the given X-nucleus with the available MR scanner. However, the different literature formulation for solenoid inductance estimation is not optimized for a wide variety of coil geometries and doesn’t take into account conductor geometry. This paper proposes an analytical method for the solenoid inductance calculation in dependence on the conductor cross-sectional geometry (flat strip and circular wire). Simulations accuracy was evaluated with workbench experimental measurement performed on a home-built strip solenoid and by comparisons with literature data referred to wire solenoids.
Electron Paramagnetic Resonance Instrumentation #DNPNMR
From The DNP-NMR Blog:
Electron Paramagnetic Resonance Instrumentation #DNPNMR
Instrumentation for DNP-NMR spectroscopy has many similar components to instrumentation for EPR spectroscopy. This is a comprehensive review of the current state-of-the-art in EPR instrumentation, covering all aspects from magnet technology, pulse generation, detection and resonator design.
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News from NMR blogs
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06-03-2020 09:31 AM
Invited Review Article: Instrumentation for nuclear magnetic resonance in zero and ultralow magnetic field
From The DNP-NMR Blog:
Invited Review Article: Instrumentation for nuclear magnetic resonance in zero and ultralow magnetic field
Tayler, Michael C. D., Thomas Theis, Tobias F. Sjolander, John W. Blanchard, Arne Kentner, Szymon Pustelny, Alexander Pines, and Dmitry Budker. “Invited Review Article: Instrumentation for Nuclear Magnetic Resonance in Zero and Ultralow Magnetic Field.” Review of Scientific Instruments 88, no. 9 (September 2017): 091101.
https://doi.org/10.1063/1.5003347.
[NMR paper] Advanced instrumentation for DNP-enhanced MAS NMR for higher magnetic fields and lower temperatures.
Advanced instrumentation for DNP-enhanced MAS NMR for higher magnetic fields and lower temperatures.
Advanced instrumentation for DNP-enhanced MAS NMR for higher magnetic fields and lower temperatures.
J Magn Reson. 2016 Mar;264:107-15
Authors: Matsuki Y, Idehara T, Fukazawa J, Fujiwara T
Abstract
Sensitivity enhancement of MAS NMR using dynamic nuclear polarization (DNP) is gaining importance at moderate fields (B090K) with potential applications in chemistry and material sciences. However, considering the ever-increasing size...
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Journal club
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02-28-2016 03:10 PM
Proton conductors: NMR solidifies fuel cells
Proton conductors: NMR solidifies fuel cells
http://www.spectroscopynow.com/common/images/thumbnails/150a48b1ae1.jpgRevealing the distribution of protons and oxygen vacancies in perovskite-type proton conductors using nuclear magnetic resonance spectroscopy could open up research to develop practical intermediate-temperature solid oxide fuel cells, according to research from Japan.
Read the rest at Spectroscopynow.com
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General
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11-01-2015 01:52 PM
[NMR images] Traditional NMR uses coils to
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http://michaelgr.com/2007/05/24/look-at-them-proteins-a-better-nuclear-magnetic-resonance-probe-and-a-look-at-computational-protein-research/
20/12/2011 4:11:48 PM GMT
Traditional NMR uses coils to
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NMR pictures
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01-12-2012 09:30 PM
[NMR photos] Inductance in an Magnetic Field
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Inductance in an Magnetic Field
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