Ziarelli, F., et al., Dynamic nuclear polarisation NMR of nanosized zirconium phosphate polymer fillers. Chemical Communications, 2014. 50(70): p. 10137-10139.
Surface functionalisation with organic modifiers of multi-layered zirconium phosphate (ZrP) nanoparticles used as polymer fillers can be directly probed by dynamic nuclear polarisation NMR, which provides unambiguous evidence of the presence of P-O-C chemical bonds at the surface of the ZrP layers, thereby confirming successful functionalisation.
Dynamic nuclear polarisation enhanced 14N overtone MAS NMR spectroscopy
From The DNP-NMR Blog:
Dynamic nuclear polarisation enhanced 14N overtone MAS NMR spectroscopy
Rossini, A., L. Emsley, and L.A. O'Dell, Dynamic nuclear polarisation enhanced 14N overtone MAS NMR spectroscopy. Phys. Chem. Chem. Phys., 2014.
http://dx.doi.org/10.1039/C4CP00590B
nmrlearner
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05-16-2014 08:06 PM
Direct Enhancement of Nuclear Singlet Order by Dynamic Nuclear Polarization
From The DNP-NMR Blog:
Direct Enhancement of Nuclear Singlet Order by Dynamic Nuclear Polarization
I don't think I posted this one already.
Tayler, M.C.D., et al., Direct Enhancement of Nuclear Singlet Order by Dynamic Nuclear Polarization. J. Am. Chem. Soc., 2012. 134(18): p. 7668-7671.
nmrlearner
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02-27-2014 03:20 AM
Cross-polarisation edited ENDOR
From The DNP-NMR Blog:
Cross-polarisation edited ENDOR
Rizzato, R., et al., Cross-polarisation edited ENDOR. Mol. Phys., 2013: p. 1-15.
http://dx.doi.org/10.1080/00268976.2013.816795
Solid state nuclear magnetic resonance with magic-angle spinning and dynamic nuclear polarization below 25K
Solid state nuclear magnetic resonance with magic-angle spinning and dynamic nuclear polarization below 25K
January 2013
Publication year: 2013
Source:Journal of Magnetic Resonance, Volume 226</br>
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We describe an apparatus for solid state nuclear magnetic resonance (NMR) with dynamic nuclear polarization (DNP) and magic-angle spinning (MAS) at 20–25K and 9.4Tesla. The MAS NMR probe uses helium to cool the sample space and nitrogen gas for MAS drive and bearings, as described earlier , but also includes a corrugated waveguide for transmission of microwaves from...
nmrlearner
Journal club
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12-15-2012 09:51 AM
Solid state nuclear magnetic resonance with magic-angle spinning and dynamic nuclear polarization below 25 K
Solid state nuclear magnetic resonance with magic-angle spinning and dynamic nuclear polarization below 25 K
Publication year: 2012
Source:Journal of Magnetic Resonance</br>
Kent R. Thurber, Alexey Potapov, Wai-Ming Yau, Robert Tycko</br>
We describe an apparatus for solid state nuclear magnetic resonance (NMR) with dynamic nuclear polarization (DNP) and magic-angle spinning (MAS) at 20-25 K and 9.4 Tesla. The MAS NMR probe uses helium to cool the sample space and nitrogen gas for MAS drive and bearings, as described earlier (Thurber et al., J. Magn. Reson. 2008) ,...
[NMR paper] Phosphate ions in bone: identification of a calcium-organic phosphate complex by 31P
Phosphate ions in bone: identification of a calcium-organic phosphate complex by 31P solid-state NMR spectroscopy at early stages of mineralization.
Related Articles Phosphate ions in bone: identification of a calcium-organic phosphate complex by 31P solid-state NMR spectroscopy at early stages of mineralization.
Calcif Tissue Int. 2003 May;72(5):610-26
Authors: Wu Y, Ackerman JL, Strawich ES, Rey C, Kim HM, Glimcher MJ
Previous 31P cross-polarization and differential cross-polarization magic angle spinning (CP/MAS and DCP/MAS) solid-state NMR...
Dynamic nuclear polarisation NMR of nanosized zirconium phosphate polymer fillers
Linear Mode
