As a habit I do not expose my iPhone to the large stray magnetic fields of high-field or unshielded NMR magnets. I do however feel safe carrying it near low-field shielded magnets with 5 Gauss stray fields within the croyostat of the magnet. That is - until lately. Last year, after topping up the liquid helium on a 300 MHz shielded magnet in a fairly small room, I noticed that my iPhone 8 had become completely unresponsive. The only stimulus it appeared to respond to was gravity. As it was under warranty, I sent it back to Apple. After a week or so, they sent it back to me with a note saying that there was nothing wrong with it. I found this very strange and did not make a connection between the helium fill and the problem with the phone. I had done many helium fills in the past while carrying an older iPhone 5. Approximately 9 months later, my iPhone 8 suffered a similar problem again after filling the same shielded 300 MHz magnet with liquid helium. This time, I took it to a local Apple Store while it was dead. The technician examined it, ran it through a software protocol, confirmed it was dead and issued me a new phone as it was in its last weeks of its warranty. Shortly after this, I read about problems others have had with iPhones and Apple watches around helium gas and finally made the connection between the problem I was having and my helium fills. Some Apple iPhones (apparently, iPhone 6 and higher) will completely die when exposed to helium gas. As if in the spirit of Easter, however, they will resurrect themselves after the helium has dissipated from the phone and the battery has been allowed to discharge. The problem is that in newer iPhones, Apple has swapped out a quartz oscillator, used in older versions of the phone, with a microelectromechanical systems chip (MEMS) which is sensitive to the presence of helium gas. This sensitivity is indeed mentioned in the User Guide of the iPhone.
Exposing iPhone to environments having high concentrations of industrial chemicals, including near evaporating liquified gasses such as helium, may damage or impair iPhone functionality. Obey all signs and instructions.
Android phones apparently do not use MEMS and therefore are not vulnerable to the problem. Several weeks ago, I absent-mindedly entered a room with my iPhone 8 while a magnet was being filled with liquid helium. Again, the same thing happened. This time, I allowed the phone to sit for a week after which I was able to charge it. After charging, it worked well with no loss of data.
Warning: If you see that a magnet is being filled with liquid helium, Do not enter the room with an iPhone 6 or higher.
[NMR paper] Investigating liquid-liquid phase separation of a monoclonal antibody using solution-state NMR spectroscopy: effect of Arg·Glu and Arg·HCl.
Investigating liquid-liquid phase separation of a monoclonal antibody using solution-state NMR spectroscopy: effect of Arg·Glu and Arg·HCl.
Investigating liquid-liquid phase separation of a monoclonal antibody using solution-state NMR spectroscopy: effect of Arg·Glu and Arg·HCl.
Mol Pharm. 2017 Jun 14;:
Authors: Kheddo P, Bramham JE, Dearman RJ, Uddin S, van der Walle CF, Golovanov AP
Abstract
Liquid-liquid phase separation (LLPS) of monoclonal antibody (mAb) formulations involves spontaneous separation into dense...
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06-15-2017 03:37 PM
Low-temperature dynamic nuclear polarization with helium-cooled samples and nitrogen-driven magic-angle spinning
From The DNP-NMR Blog:
Low-temperature dynamic nuclear polarization with helium-cooled samples and nitrogen-driven magic-angle spinning
Thurber, K. and R. Tycko, Low-temperature dynamic nuclear polarization with helium-cooled samples and nitrogen-driven magic-angle spinning. J Magn Reson, 2016. 264: p. 99-106.
http://www.ncbi.nlm.nih.gov/pubmed/26920835
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04-11-2016 07:16 PM
Low-temperature dynamic nuclear polarization with helium-cooled samples and nitrogen-driven magic-angle spinning
Low-temperature dynamic nuclear polarization with helium-cooled samples and nitrogen-driven magic-angle spinning
Publication date: March 2016
Source:Journal of Magnetic Resonance, Volume 264</br>
Author(s): Kent Thurber, Robert Tycko</br>
We describe novel instrumentation for low-temperature solid state nuclear magnetic resonance (NMR) with dynamic nuclear polarization (DNP) and magic-angle spinning (MAS), focusing on aspects of this instrumentation that have not been described in detail in previous publications. We characterize the performance of an extended...
SpinDrops for ipad and iphones
SpinDrops for ipad and iphones
SpinDrops allows students and scientists in physics, chemistry, biochemistry and medicine to explore and to better understand basic and advanced magnetic resonance experiments.
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An apparatus for pulsed ESR and DNP experiments using optically excited triplet states down to liquid helium temperatures
From The DNP-NMR Blog:
An apparatus for pulsed ESR and DNP experiments using optically excited triplet states down to liquid helium temperatures
Eichhorn, T.R., et al., An apparatus for pulsed ESR and DNP experiments using optically excited triplet states down to liquid helium temperatures. J. Magn. Reson., 2013. 234(0): p. 58-66.
http://dx.doi.org/10.1016/j.jmr.2013.06.009
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08-30-2013 04:35 PM
[U. of Ottawa NMR Facility Blog] Resolution During a Liquid Helium Refill
Resolution During a Liquid Helium Refill
Students sometimes ask whether or not they can collect NMR data during a liquid helium refill. The answer depends on the type of NMR experiment. For most solids experiments, where high resolution (