Dynamic nuclear polarization (DNP)-enhanced solid-state NMR spectroscopy under magic-angle spinning has recently emerged as a unique analytical method to probe surfaces at atomic resolution. In this article, we first describe the basic principles of dynamic nuclear polarization surface enhanced NMR spectroscopy (DNP SENS). The article continues with a large review of recent literature that illustrates the versatility of this technique and its incredible potential to reveal new structural features at surfaces with details at an unprecedented level. The most recent developments, such as the application of DNP SENS to highly reactive surface sites, are finally covered.
Surface chemical heterogeneity modulates silica surface hydration #DNPNMR #ODNP
From The DNP-NMR Blog:
Surface chemical heterogeneity modulates silica surface hydration #DNPNMR #ODNP
Schrader, Alex M., Jacob I. Monroe, Ryan Sheil, Howard A. Dobbs, Timothy J. Keller, Yuanxin Li, Sheetal Jain, M. Scott Shell, Jacob N. Israelachvili, and Songi Han. “Surface Chemical Heterogeneity Modulates Silica Surface Hydration.” Proceedings of the National Academy of Sciences 115, no. 12 (March 20, 2018): 2890–95.
https://doi.org/10.1073/pnas.1722263115.
nmrlearner
News from NMR blogs
0
03-24-2019 10:41 PM
Recent advances in application of 27Al NMR spectroscopy to materials science
Recent advances in application of 27Al NMR spectroscopy to materials science
Publication date: May 2016
Source:Progress in Nuclear Magnetic Resonance Spectroscopy, Volumes 94–95</br>
Author(s): Mohamed Haouas, Francis Taulelle, Charlotte Martineau</br>
Valuable information about the local environment of the aluminum nucleus can be obtained through 27Al Nuclear Magnetic Resonance (NMR) parameters like the isotropic chemical shift, scalar and quadrupolar coupling constants, and relaxation rate. With nearly 250 scientific articles per year dealing with 27Al NMR...
nmrlearner
Journal club
0
04-09-2016 03:54 AM
[Stan NMR blog] Materials Science and Technology books
Materials Science and Technology books
Books directory: A large list of books about Materials with links to Amazon.
Source: Stan blog library
nmrlearner
News from NMR blogs
0
03-05-2012 04:29 PM
[Stan NMR blog] Materials Science and Technology books
Materials Science and Technology books
BOOKS LIST: A huge collection with links to Amazon.
Source: Stan blog library
nmrlearner
News from NMR blogs
0
03-03-2012 01:39 AM
24th Canadian Materials Science Conference – call for abstracts
24th Canadian Materials Science Conference – call for abstracts
We invite you to submit an abstract for presentation at the 24th CMSC, Materials: Atoms to Applications, which will be held at The University of Western Ontario, June 5-8, 2012. We are accepting abstracts for both oral and poster presentations; priority will be given to submissions by students.
The Conference has been expanded from its roots in metallurgy to include presentations related to many materials including bio- and nano-materials and composites; a somewhat more detailed list is shown on the attached flyer which we...
Fast Characterization of Functionalized Silica Materials by Silicon-29 Surface-Enhanced NMR Spectroscopy Using Dynamic Nuclear Polarization
Fast Characterization of Functionalized Silica Materials by Silicon-29 Surface-Enhanced NMR Spectroscopy Using Dynamic Nuclear Polarization
Moreno Lelli, David Gajan, Anne Lesage, Marc A. Caporini, Veronika Vitzthum, Pascal Mie?ville, Florent He?roguel, Fernando Rasco?n, Arthur Roussey, Chloe? Thieuleux, Malika Boualleg, Laurent Veyre, Geoffrey Bodenhausen, Christophe Cope?ret and Lyndon Emsley
http://pubs.acs.org/appl/literatum/publisher/achs/journals/content/jacsat/0/jacsat.ahead-of-print/ja110791d/aop/images/medium/ja-2010-10791d_0005.gif
Journal of the American Chemical Society...