Cross polarization from (1)H to quadrupolar (6)Li nuclei for dissolution DNP

		BioNMR > NMR community > News from NMR blogs
Cross polarization from (1)H to quadrupolar (6)Li nuclei for dissolution DNP

Webservers

NMR processing:

MDD

NMR assignment:

Backbone:

Side-chains:

NOEs:

Structure from NMR restraints:

Ab initio:

Fragment-based:

Rosetta-NMR (Robetta)

Template-based:

GeNMR

I-TASSER

Refinement:

Amber

Structure from chemical shifts:

Fragment-based:

Homology-based:

Torsion angles from chemical shifts:

Preditor

TALOS

Promega- Proline

Secondary structure from chemical shifts:

CSI (via RCI server)

TALOS

MICS caps, β-turns

d2D

PECAN

Flexibility from chemical shifts:

RCI

Interactions from chemical shifts:

HADDOCK

Chemical shifts re-referencing:

NMR model quality:

NOEs, other restraints:

Chemical shifts:

RDCs:

Pseudocontact shifts:

Protein geomtery:

SAVES2 or SAVES4

Quality Control Check

NMR spectrum prediction:

FANDAS

MestReS

V-NMR

Flexibility from structure:

Backbone S2

Methyl S2

B-factor

Molecular dynamics:

Gromacs

Amber

Antechamber

Chemical shifts prediction:

From structure:

Shiftx2

Sparta+

Camshift

CH3shift- Methyl

ArShift- Aromatic

ShiftS

Proshift

PPM

CheShift-2- Cα

From sequence:

Shifty

Camcoil

Poulsen_rc_CS

Disordered proteins:

MAXOCC

Format conversion & validation:

CCPN

From NMR-STAR 3.1

Validate NMR-STAR 3.1

NMR sample preparation:

Protein disorder:

DisMeta

Protein solubility:

Isotope labeling:

Solid-state NMR:

Thread Tools

Search this Thread

Rate Thread

Display Modes

11-05-2014, 04:04 PM

nmrlearner

Senior Member

Join Date: Jan 2005

Posts: 23,732

Points: 193,617, Level: 100

Level up: 0%, 0 Points needed

Activity: 50.7%

Last Achievements

Award-Showcase

NMR Credits: 0

NMR Points: 193,617

Downloads: 0

Uploads: 0

Cross polarization from (1)H to quadrupolar (6)Li nuclei for dissolution DNP

From The DNP-NMR Blog:

Cross polarization from (1)H to quadrupolar (6)Li nuclei for dissolution DNP

Perez Linde, A.J., et al., Cross polarization from (1)H to quadrupolar (6)Li nuclei for dissolution DNP. Phys Chem Chem Phys, 2014. 16(45): p. 24813-7.

http://www.ncbi.nlm.nih.gov/pubmed/25319311

Cross polarization from protons to quadrupolar (6)Li nuclei is combined with dynamic nuclear polarization of protons at 1.2 K and 6.7 T using TEMPOL as a polarizing agent followed by rapid dissolution. Compared to direct (6)Li DNP without cross-polarization, a higher nuclear spin polarization P((6)Li) can be obtained in a shorter time. A double resonance (1)H-(6)Li probe was designed that is equipped for Longitudinally Detected Electron Spin Resonance.

Go to The DNP-NMR Blog for more info.

Did you find this post helpful?

Similar Threads
Thread	Thread Starter	Forum	Replies	Last Post
Cross-polarization for dissolution dynamic nuclear polarization From The DNP-NMR Blog: Cross-polarization for dissolution dynamic nuclear polarization Batel, M., et al., Cross-polarization for dissolution dynamic nuclear polarization. Phys Chem Chem Phys, 2014. 16(39): p. 21407-16. http://www.ncbi.nlm.nih.gov/pubmed/25182534	nmrlearner	News from NMR blogs	0	10-08-2014 05:52 PM
Cross Polarization for Dissolution Dynamic Nuclear Polarization From The DNP-NMR Blog: Cross Polarization for Dissolution Dynamic Nuclear Polarization Batel, M., et al., Cross Polarization for Dissolution Dynamic Nuclear Polarization. Phys. Chem. Chem. Phys., 2014. http://dx.doi.org/10.1039/C4CP02696A	nmrlearner	News from NMR blogs	0	08-22-2014 07:27 PM
Hyperpolarization of deuterated metabolites via remote cross-polarization and dissolution dynamic nuclear polarization From The DNP-NMR Blog: Hyperpolarization of deuterated metabolites via remote cross-polarization and dissolution dynamic nuclear polarization Vuichoud, B., et al., Hyperpolarization of deuterated metabolites via remote cross-polarization and dissolution dynamic nuclear polarization. J Phys Chem B, 2014. 118(5): p. 1411-5. http://www.ncbi.nlm.nih.gov/pubmed/24397585	nmrlearner	News from NMR blogs	0	04-02-2014 11:54 PM
Cross Polarization for Dissolution Dynamic Nuclear Polarization Experiments at Readily Accessible Temperatures 1.2* From The DNP-NMR Blog: Cross Polarization for Dissolution Dynamic Nuclear Polarization Experiments at Readily Accessible Temperatures 1.2*	nmrlearner	News from NMR blogs	0	11-21-2013 01:14 AM
NMR of Quadrupolar Nuclei in Solid Materials NMR of Quadrupolar Nuclei in Solid Materials http://media.wiley.com/product_data/coverImage/86/04709739/0470973986.jpgOver the past 20 years technical developments in superconducting magnet technology and instrumentation have increased the potential of NMR spectroscopy so that it is now possible to study a wide range of solid materials. In addition, one can probe the nuclear environments of many other additional atoms that possess the property of spin. In particular, it is possible to carry out NMR experiments on isotopes that have nuclear spin greater that ½ (i.e. quadrupolar...	nmrlearner	Books	0	02-03-2013 09:00 AM
Enhanced Solid-State NMR Correlation Spectroscopy of Quadrupolar Nuclei Using Dynamic Nuclear Polarization Enhanced Solid-State NMR Correlation Spectroscopy of Quadrupolar Nuclei Using Dynamic Nuclear Polarization Daniel Lee, Hiroki Takahashi, Aany S. L. Thankamony, Jean-Philippe Dacquin, Michel Bardet, Olivier Lafon and Gae?l De Pae?pe http://pubs.acs.org/appl/literatum/publisher/achs/journals/content/jacsat/0/jacsat.ahead-of-print/ja307755t/aop/images/medium/ja-2012-07755t_0004.gif Journal of the American Chemical Society DOI: 10.1021/ja307755t http://feeds.feedburner.com/~ff/acs/jacsat?d=yIl2AUoC8zA http://feeds.feedburner.com/~r/acs/jacsat/~4/NcXbDBD9aBc	nmrlearner	Journal club	0	11-03-2012 03:56 PM
[NMR900 blog] New book: NMR of Quadrupolar Nuclei in Solid Materials New book: NMR of Quadrupolar Nuclei in Solid Materials edited by Roderick E. Wasylishen, Sharon E. Ashbrook, Stephen Wimperis Hardcover: 550 pages Publisher: Wiley; August 2012 Language: English ISBN: 978-0470973981 http://www.amazon.com/dp/0470973986 http://www.amazon.ca/dp/0470973986	nmrlearner	News from NMR blogs	0	08-09-2012 08:10 AM
Rapid Solid-State NMR of Deuterated Proteins by Interleaved Cross-Polarization fromH andH Nuclei Rapid Solid-State NMR of Deuterated Proteins by Interleaved Cross-Polarization fromH andH Nuclei Publication year: 2011 Source: Journal of Magnetic Resonance, Available online 9 November 2011</br> MortenBjerring, BeritPaaske, HartmutOschkinat, UmitAkbey, Niels Chr.*Nielsen</br> We present a novel sampling strategy, interleaving acquisition of multiple NMR spectra by exploiting initial polarization subsequently fromH andH spins, taking advantage of their differentT1relaxation times. DifferentH- andH-polarization based spectra are in this way simultaneously recorded improving either...	nmrlearner	Journal club	0	11-10-2011 07:38 AM

« Previous Thread | Next Thread »

Posting Rules
You may not post new threads You may not post replies You may not post attachments You may not edit your posts BB code is On Smilies are On [IMG] code is On HTML code is Off Trackbacks are Off Pingbacks are Off Refbacks are Off