Annabestani, Razieh, Maryam Mirkamali, and Raffi Budakian. “Adiabatic-NOVEL for Nano-Scale Magnetic Resonance Imaging.” ArXiv:1712.09128 [Quant-Ph], December 25, 2017.
We propose a highly efficient dynamic nuclear polarization technique that is robust against field in-homogeneity. This technique is designed to enhance the detection sensitivity in nano-MRI, where large Rabi field gradients are required. The proposed technique consists of an adiabatic half passage pulse followed by an adiabatic linear sweep of the electron Rabi frequency and can be considered as an adiabatic version of nuclear orientation via electron spin locking (adiabatic-NOVEL). We analyze the spin dynamics of an electron-nuclear system that is under microwave irradiation at high static magnetic field and at cryogenic temperature. The result shows that an amplitude modulation of the microwave field makes adiabatic-NOVEL highly efficient and robust against both the static and microwave field in-homogeneity.
Electron spin resonance studies on deuterated nitroxyl spin probes used in Overhauser-enhanced magnetic resonance imaging #DNPNMR #ODNP
From The DNP-NMR Blog:
Electron spin resonance studies on deuterated nitroxyl spin probes used in Overhauser-enhanced magnetic resonance imaging #DNPNMR #ODNP
Jebaraj, D. David, Hideo Utsumi, and A. Milton Franklin Benial. “Electron Spin Resonance Studies on Deuterated Nitroxyl Spin Probes Used in Overhauser-Enhanced Magnetic Resonance Imaging.” Magnetic Resonance in Chemistry 55, no. 8 (2017): 700–705.
https://doi.org/10.1002/mrc.4576.
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06-23-2018 12:47 AM
ESR line width and line shape dependence of Overhauser-enhanced magnetic resonance imaging #DNPNMR
From The DNP-NMR Blog:
ESR line width and line shape dependence of Overhauser-enhanced magnetic resonance imaging #DNPNMR
Meenakumari, V., Hideo Utsumi, A. Jawahar, and A. Milton Franklin Benial. “ESR Line Width and Line Shape Dependence of Overhauser-Enhanced Magnetic Resonance Imaging.” Magnetic Resonance in Chemistry 54, no. 11 (2016): 874–79.
https://doi.org/10.1002/mrc.4489
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06-13-2018 05:09 PM
[NMR paper] Progress in proton-detected solid-state NMR (SSNMR): Super-fast 2D SSNMR collection for nano-mole-scale proteins.
Progress in proton-detected solid-state NMR (SSNMR): Super-fast 2D SSNMR collection for nano-mole-scale proteins.
Progress in proton-detected solid-state NMR (SSNMR): Super-fast 2D SSNMR collection for nano-mole-scale proteins.
J Magn Reson. 2017 Nov 28;286:99-109
Authors: Ishii Y, Wickramasinghe A, Matsuda I, Endo Y, Ishii Y, Nishiyama Y, Nemoto T, Kamihara T
Abstract
Proton-detected solid-state NMR (SSNMR) spectroscopy has attracted much attention due to its excellent sensitivity and effectiveness in the analysis of trace...
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12-11-2017 12:45 PM
[NMR paper] Progress in Proton-detected Solid-state NMR (SSNMR): Super-fast 2D SSNMR Collection for Nano-mole-scale Proteins
Progress in Proton-detected Solid-state NMR (SSNMR): Super-fast 2D SSNMR Collection for Nano-mole-scale Proteins
Publication date: Available online 28 November 2017
Source:Journal of Magnetic Resonance</br>
Author(s): Yoshitaka Ishii, Ayesha Wickramasinghe, Isamu Matsuda, Yuki Endo, Yuji Ishii, Yusuke Nishiyama, Takahiro Nemoto, Takayuki Kamihara</br>
Proton-detected solid-state NMR (SSNMR) spectroscopy has attracted much attention due to its excellent sensitivity and effectiveness in the analysis of trace amounts of amyloid proteins and other...
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11-29-2017 09:22 AM
Simultaneous and spectroscopic redox molecular imaging of multiple free radical intermediates using dynamic nuclear polarization-magnetic resonance imaging #DNPNMR
From The DNP-NMR Blog:
Simultaneous and spectroscopic redox molecular imaging of multiple free radical intermediates using dynamic nuclear polarization-magnetic resonance imaging #DNPNMR
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Hyodo, F., et al., Simultaneous and spectroscopic redox molecular imaging of multiple free radical intermediates using dynamic nuclear polarization-magnetic resonance imaging. Anal Chem, 2014. 86(15): p. 7234-8.
https://www.ncbi.nlm.nih.gov/pubmed/25036767
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08-17-2017 12:56 AM
Dissolution dynamic nuclear polarization–enhanced magnetic resonance spectroscopy and imaging: Chemical and biochemical reactions in nonequilibrium conditions #DNPNMR
From The DNP-NMR Blog:
Dissolution dynamic nuclear polarization–enhanced magnetic resonance spectroscopy and imaging: Chemical and biochemical reactions in nonequilibrium conditions #DNPNMR
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Lee, Y., Dissolution dynamic nuclear polarization–enhanced magnetic resonance spectroscopy and imaging: Chemical and biochemical reactions in nonequilibrium conditions. Applied Spectroscopy Reviews, 2015. 51(3): p. 210-226.
https://doi.org/10.1080/05704928.2015.1116078
[NMR paper] Nano-mole scale sequential signal assignment by (1)H-detected protein solid-state NMR.
Nano-mole scale sequential signal assignment by (1)H-detected protein solid-state NMR.
Related Articles Nano-mole scale sequential signal assignment by (1)H-detected protein solid-state NMR.
Chem Commun (Camb). 2015 Aug 28;
Authors: Wang S, Parthasarathy S, Xiao Y, Nishiyama Y, Long F, Matsuda I, Endo Y, Nemoto T, Yamauchi K, Asakura T, Takeda M, Terauchi T, Kainosho M, Ishii Y
Abstract
We present a 3D (1)H-detected solid-state NMR (SSNMR) approach for main-chain signal assignments of 10-100 nmol of fully protonated proteins...