Publication date: Available online 3 January 2016 Source:Comptes Rendus Chimie
Author(s): Yang Li, David G. Reid, Dominique Bazin, Michel Daudon, Melinda J. Duer
Solid state NMR (ssNMR) can characterize mineral (31P) and organic (13C) components of human salivary stones (n*=*8). All show apatitic 31P spectra. 13C ssNMR indicates more protein, of more consistent composition, than apatitic uroliths, with prominent signals from Tyr, Phe, and His. Citrate and lipids, identified by dipolar dephasing (DD), and polysaccharides are also observable in varying amounts. 13C{31P} rotational echo double resonance (13C{31P} REDOR) identifies carbon atoms in close (
[NMR paper] ?-(S)-Trifluoromethyl proline: evaluation as a structural substitute of proline for solid state (19)F-NMR peptide studies.
?-(S)-Trifluoromethyl proline: evaluation as a structural substitute of proline for solid state (19)F-NMR peptide studies.
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Abstract
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Sci Rep. 2013;3:2913
Authors: Ogura K, Okamura H
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Structure and Interactions of Plant Cell-Wall Polysaccharides by Two- and Three-Dimensional Magic-Angle-Spinning Solid-State NMR
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http://pubs.acs.org/appl/literatum/publisher/achs/journals/content/bichaw/0/bichaw.ahead-of-print/bi101795q/aop/images/medium/bi-2010-01795q_0008.gif
Biochemistry
DOI: 10.1021/bi101795q
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Biochem J. 1996 May 1;315 ( Pt 3):833-44
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