[Question from NMRWiki Q&A forum] 1H t2 measurement in solid state nmr
1H t2 measurement in solid state nmr
How to measure t2 of 1H in solid state nmr? we use saturation burst followed by cp to measure T1 of 1H in solid state indirectly.
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News from other NMR forums
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02-29-2012 10:32 PM
Revealing Protein Structures in Solid-Phase Peptide Synthesis by 13C Solid-State NMR: Evidence of Excessive Misfolding for Alzheimer’s ?
Revealing Protein Structures in Solid-Phase Peptide Synthesis by 13C Solid-State NMR: Evidence of Excessive Misfolding for Alzheimer’s ?
Songlin Wang and Yoshitaka Ishii
http://pubs.acs.org/appl/literatum/publisher/achs/journals/content/jacsat/0/jacsat.ahead-of-print/ja212190z/aop/images/medium/ja-2011-12190z_0002.gif
Journal of the American Chemical Society
DOI: 10.1021/ja212190z
http://feeds.feedburner.com/~ff/acs/jacsat?d=yIl2AUoC8zA
http://feeds.feedburner.com/~r/acs/jacsat/~4/6EE7uthrnLg
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01-31-2012 08:34 PM
[Question from NMRWiki Q&A forum] about sideband in solid-state NMR
about sideband in solid-state NMR
Hi, dear all,
I've encounter a strange phenomemon.While the target speed of MAS was set to be 12kHz, the sidebands of 6kHz difference with respect to the center peak arised.What may cause the problem? Is there any possibility that the real speed is half of the displayed speed?
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[NMR900 blog] Solid-State DNP-NMR Spectrometer at Guelph
Solid-State DNP-NMR Spectrometer at Guelph
Bruker has announced that the first commercial 395 GHz solid-state DNP-NMR spectrometer (600 MHz) will be installed at the University of Guelph (read the full press-release). https://blogger.googleusercontent.com/tracker/8663203727601106205-8346694996229720249?l=nmr900.blogspot.com
Read complete story on NMR900 blog
nmrlearner
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04-13-2011 01:15 AM
[Question from NMRWiki Q&A forum] optimising o1 in solid state nmr
optimising o1 in solid state nmr
I'm a little bit confused about setting o1, in the case of a solid sample First o1 is the offset of the transmitter frequency so sfo1 = BF1 + o1In my case I have to set Sfo1 = BF1 so I must set o1 = 0 HzSecond there is another way to optimize o1 whish is by applying gs and looking the fid, adjusting o1 until we have a good exponential decrease of the fid. In this case o1 value may not be 0 Hz.Does the second technique is valid in solid stat experiences?And which one I have to use?
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nmrlearner
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03-09-2011 04:19 AM
[NMR paper] Solid-state NMR studies of the membrane-bound closed state of the colicin E1 channel
Solid-state NMR studies of the membrane-bound closed state of the colicin E1 channel domain in lipid bilayers.
Related Articles Solid-state NMR studies of the membrane-bound closed state of the colicin E1 channel domain in lipid bilayers.
Protein Sci. 1998 Feb;7(2):342-8
Authors: Kim Y, Valentine K, Opella SJ, Schendel SL, Cramer WA
The colicin E1 channel polypeptide was shown to be organized anisotropically in membranes by solid-state NMR analysis of samples of uniformly 15N-labeled protein in oriented planar phospholipid bilayers. The 190...
Solid-State NMR Crystallographythrough ParamagneticRestraints
Linear Mode
