Heteronuclear ^(13)C-^(15)N couplings were measured in single-scan nuclear magnetic resonance (NMR) experiments for a variety of nitrogen-containing chemical compounds with varied structural characteristics, by using a one-dimensional (1D) ^(13)C-^(15)N multiple-quantum (MQ)-filtered experiment. Sensitivity limitations of the MQ filtering were overcome by the combined use of ^(15)N labeling and dissolution dynamic nuclear polarization (dDNP), performed at cryogenic conditions and followed by...
Dipolar Order Mediated 1H -> 13C Cross-Polarization for Dissolution-Dynamic Nuclear Polarization #DNPNMR
From The DNP-NMR Blog:
Dipolar Order Mediated 1H -> 13C Cross-Polarization for Dissolution-Dynamic Nuclear Polarization #DNPNMR
Elliott, Stuart J., Samuel F. Cousin, Quentin Chappuis, Olivier Cala, Morgan Ceillier, Aurélien Bornet, and Sami Jannin. “Dipolar Order Mediated 1H -> 13C Cross-Polarization for Dissolution-Dynamic Nuclear Polarization.” Preprint. Hyperpolarization/Pulse-sequence development, February 20, 2020.
https://doi.org/10.5194/mr-2020-4
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04-29-2020 04:16 PM
Hyperpolarization of nitrogen-15 nuclei by cross polarization and dissolution dynamic nuclear polarization
From The DNP-NMR Blog:
Hyperpolarization of nitrogen-15 nuclei by cross polarization and dissolution dynamic nuclear polarization
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Milani, J., et al., Hyperpolarization of nitrogen-15 nuclei by cross polarization and dissolution dynamic nuclear polarization. Review of Scientific Instruments, 2017. 88(1): p. 015109.
http://dx.doi.org/10.1063/1.4973777
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09-04-2017 03:11 PM
Dissolution dynamic nuclear polarization–enhanced magnetic resonance spectroscopy and imaging: Chemical and biochemical reactions in nonequilibrium conditions #DNPNMR
From The DNP-NMR Blog:
Dissolution dynamic nuclear polarization–enhanced magnetic resonance spectroscopy and imaging: Chemical and biochemical reactions in nonequilibrium conditions #DNPNMR
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Lee, Y., Dissolution dynamic nuclear polarization–enhanced magnetic resonance spectroscopy and imaging: Chemical and biochemical reactions in nonequilibrium conditions. Applied Spectroscopy Reviews, 2015. 51(3): p. 210-226.
https://doi.org/10.1080/05704928.2015.1116078
Polarization Transfer from Ligands Hyperpolarized by Dissolution Dynamic Nuclear Polarization for Screening in Drug Discovery
From The DNP-NMR Blog:
Polarization Transfer from Ligands Hyperpolarized by Dissolution Dynamic Nuclear Polarization for Screening in Drug Discovery
Min, H., G. Sekar, and C. Hilty, Polarization Transfer from Ligands Hyperpolarized by Dissolution Dynamic Nuclear Polarization for Screening in Drug Discovery. ChemMedChem, 2015. 10(9): p. 1559-63.
http://www.ncbi.nlm.nih.gov/pubmed/26315550
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10-05-2015 07:08 PM
Hyperpolarization of deuterated metabolites via remote cross-polarization and dissolution dynamic nuclear polarization
From The DNP-NMR Blog:
Hyperpolarization of deuterated metabolites via remote cross-polarization and dissolution dynamic nuclear polarization
Vuichoud, B., et al., Hyperpolarization of deuterated metabolites via remote cross-polarization and dissolution dynamic nuclear polarization. J Phys Chem B, 2014. 118(5): p. 1411-5.
http://www.ncbi.nlm.nih.gov/pubmed/24397585
Single-Scan Heteronuclear (13)C-(15)N J-Coupling NMR Observations Enhanced by Dissolution Dynamic Nuclear Polarization
Linear Mode
