[NMR paper] NMR Structural Biology of Sulfated Glycans.
NMR Structural Biology of Sulfated Glycans.
Related Articles NMR Structural Biology of Sulfated Glycans.
J Biomol Struct Dyn. 2016 May 11;:1-45
Authors: Soares PA, Queiroz IN, Pomin VH
Abstract
Sulfated fucans, sulfated galactans and glycosaminoglycans are extensively studied worldwide in terms of both structure and biomedical functions. Liquid-state nuclear magnetic resonance (NMR) spectroscopy is the most employed analytical technique in structural analysis of these sulfated glycans. This is due to the fact that NMR-based...
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05-12-2016 09:30 PM
[NMR paper] NMR of glycans: Shedding new light on old problems.
NMR of glycans: Shedding new light on old problems.
NMR of glycans: Shedding new light on old problems.
Prog Nucl Magn Reson Spectrosc. 2014 May;79C:48-68
Authors: Battistel MD, Azurmendi HF, Yu B, Freedberg DI
Abstract
The diversity in molecular arrangements and dynamics displayed by glycans renders traditional NMR strategies, employed for proteins and nucleic acids, insufficient. Because of the unique properties of glycans, structural studies often require the adoption of a different repertoire of tailor-made experiments and...
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05-13-2014 03:11 PM
NMR of Glycans: Shedding New Light on Old Problems
NMR of Glycans: Shedding New Light on Old Problems
Publication date: Available online 14 February 2014
Source:Progress in Nuclear Magnetic Resonance Spectroscopy</br>
Author(s): Marcos D. Battistel , Hugo F. Azurmendi , Bingwu Yu , Darón I. Freedberg</br>
The diversity in molecular arrangements and dynamics displayed by glycans renders traditional NMR strategies, employed for proteins and nucleic acids, insufficient. Because of the unique properties of glycans, structural studies often require the adoption of a different repertoire of tailor-made experiments...
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02-15-2014 07:22 AM
Journal Highlight: Quantitative NMR: An applicable method for quantitative analysis of medicinal plant extracts and herbal products
Journal Highlight: Quantitative NMR: An applicable method for quantitative analysis of medicinal plant extracts and herbal products
http://www.spectroscopynow.com/common/images/thumbnails/13abcca009b.jpgA quantitative NMR method has been reported for quantitative analysis of three medicinal plant extracts and their herbal products without the need of authentic standards.
Source: Spectroscopynow.com
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02-03-2013 08:49 AM
A rigid disulfide-linked nitroxide side chain simplifies the quantitative analysis of PRE data
A rigid disulfide-linked nitroxide side chain simplifies the quantitative analysis of PRE data
Abstract The measurement of 1H transverse paramagnetic relaxation enhancement (PRE) has been used in biomolecular systems to determine long-range distance restraints and to visualize sparsely-populated transient states. The intrinsic flexibility of most nitroxide and metal-chelating paramagnetic spin-labels, however, complicates the quantitative interpretation of PREs due to delocalization of the paramagnetic center. Here, we present a novel, disulfide-linked nitroxide spin label, R1p, as...
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09-30-2011 08:01 PM
[NMR paper] Detection of conserved N-linked glycans and phase-variable lipooligosaccharides and c
Detection of conserved N-linked glycans and phase-variable lipooligosaccharides and capsules from campylobacter cells by mass spectrometry and high resolution magic angle spinning NMR spectroscopy.
Related Articles Detection of conserved N-linked glycans and phase-variable lipooligosaccharides and capsules from campylobacter cells by mass spectrometry and high resolution magic angle spinning NMR spectroscopy.
J Biol Chem. 2003 Jul 4;278(27):24509-20
Authors: Szymanski CM, Michael FS, Jarrell HC, Li J, Gilbert M, Larocque S, Vinogradov E, Brisson JR
...
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11-24-2010 09:01 PM
On the measurement of 15N-{1H} nuclear Overhauser effects. 2. Effects of the saturati
On the measurement of 15N-{1H} nuclear Overhauser effects. 2. Effects of the saturation scheme and water signal suppression
Publication year: 2010
Source: Journal of Magnetic Resonance, In Press, Accepted Manuscript, Available online 24 September 2010</br>
Fabien, Ferrage , Amy, Reichel , Shibani, Battacharya , David, Cowburn , Ranajeet, Ghose</br>
Measurement of steady-state 15N-{1H} nuclear Overhauser effects forms a cornerstone of most methods to determine protein backbone dynamics from spin-relaxation data, since it is the most reliable probe of very fast motions on the ps-ns...
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09-25-2010 07:47 AM
[NMR paper] The effects of proteins on [Ca2+] measurement: different effects on fluorescent and N
The effects of proteins on measurement: different effects on fluorescent and NMR methods.
http://www.ncbi.nlm.nih.gov/corehtml/query/egifs/http:--linkinghub.elsevier.com-ihub-images-PubMedLink.gif Related Articles The effects of proteins on measurement: different effects on fluorescent and NMR methods.
Cell Calcium. 1996 Nov;20(5):425-30
Authors: Matsuda S, Kusuoka H, Hashimoto K, Tsujimura E, Nishimura T
Previous reports showed that the presence of proteins shifts the apparent dissociation constant (Kd) of a fluorescent dye indicator to...