Abstract
The review articles published in "Progress in NMR Spectroscopy" are usually invited treatments of topics of current interest, but occasionally the Editorial Board may take an initiative to publish important historical material that is not widely available. The present article represents just such a case. Jean Jeener gave a lecture in 1971 at a summer school in Basko Polje, in what was then called Yugoslavia. As is now widely known, Jean Jeener laid down the foundations in that lecture of two - and higher - dimensional NMR spectroscopy by proposing the homonuclear COSY experiment. Jeener realized that the new proposal would open the door towards protein NMR and molecular structure determinations, but he felt that useful versions of such experiments could not be achieved with the NMR, computer and electronics technology available at that time, so that copies of the lecture notes were circulated (the Basko Polje lecture notes by J. Jeener and G. Alewaeters), but no formal publication followed. Fortunately, Ernst, Freeman, Griffin, and many others were more far-sighted and optimistic. An early useful extension was Ernst's proposal to replace the original projection/reconstruction technique of MRI by the widely adopted Fourier transform method inspired by the Basko Polje lecture. Later, the pulse method spread over many fields of spectroscopy as soon as the required technology became available. Jean Jeener, Emeritus professor, Université Libre de Bruxelles. Geoffrey Bodenhausen, Ecole Normale Supérieure, Paris.
Pulse pair technique in high resolution NMR”; a reprint of the historical 1971 lecture notes on two dimensional spectroscopy
Pulse pair technique in high resolution NMR”; a reprint of the historical 1971 lecture notes on two dimensional spectroscopy
Publication date: Available online 12 April 2016
Source:Progress in Nuclear Magnetic Resonance Spectroscopy</br>
Author(s): Jean Jeener, Geoffrey Bodenhausen</br>
The review articles published in “Progress in NMR Spectroscopy” are usually invited treatments of topics of current interest, but occasionally the Editorial Board may take an initiative to publish important historical material that is not widely available. The present article...
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04-15-2016 02:48 AM
[NMR paper] "In-plant" NMR: Analysis of the Intact Plant Vesicularia dubyana by High Resolution NMR Spectroscopy.
"In-plant" NMR: Analysis of the Intact Plant Vesicularia dubyana by High Resolution NMR Spectroscopy.
"In-plant" NMR: Analysis of the Intact Plant Vesicularia dubyana by High Resolution NMR Spectroscopy.
Molecules. 2015;20(3):4359-4368
Authors: Kutyshenko VP, Beskaravayny P, Uversky VN
Abstract
We present here the concept of "in-plant" NMR and show that high-resolution NMR spectroscopy is suitable for the analysis of intact plants and can be used to follow the changes in the intraorganismal molecular composition over long time...
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03-12-2015 10:33 AM
Postdoctoral positions "high field ?MAS-DNP- NMR” and “Rapid melt DNP"
From The DNP-NMR Blog:
Postdoctoral positions "high field ?MAS-DNP- NMR” and “Rapid melt DNP"
Two postdoc positions for “DNP-enhanced NMR” both in the solid and liquid state are available immediately at the Solid State NMR group of the Institute of Molecules and Materials at the Radboud University of Nijmegen.
The solid NMR group at the Radboud University specializes in developing innovative technology to perform NMR spectroscopy on very small samples volumes both in the solid and in the liquid state. In the solid phase one can obtain ultrahigh proton decoupling fields (above 1...
High dimensional and high resolution pulse sequences for backbone resonance assignment of intrinsically disordered proteins
High dimensional and high resolution pulse sequences for backbone resonance assignment of intrinsically disordered proteins
Abstract Four novel 5D (HACA(N)CONH, HNCOCACB, (HACA)CON(CA)CONH, (H)NCO(NCA)CONH), and one 6D ((H)NCO(N)CACONH) NMR pulse sequences are proposed. The new experiments employ non-uniform sampling that enables achieving high resolution in indirectly detected dimensions. The experiments facilitate resonance assignment of intrinsically disordered proteins. The novel pulse sequences were successfully tested using δ subunit (20 kDa) of Bacillus subtilis RNA polymerase...
"Pulse pair technique in high resolution NMR" a reprint of the historical 1971 lecture notes on two-dimensional spectroscopy.
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