Publication date: Available online 4 August 2016 Source:Progress in Nuclear Magnetic Resonance Spectroscopy
Author(s): Kaustubh R. Mote, Vipin Agarwal, P.K. Madhu
It has been slightly more than fifty years since the first homonuclear spin decoupling scheme, Lee-Goldburg decoupling, was proposed for removing homonuclear dipolar interactions in solid-state nuclear magnetic resonance. A family of such schemes has made observation of high-resolution NMR spectra of abundant spins possible in various applications in solid state. This review outlines the strategies used in this field and the future prospects of homonuclear spin decoupling in solid-state NMR. Graphical abstract
Homonuclear decoupling for spectral simplification of carbon-13 enriched molecules in solution-state NMR enhanced by dissolution DNP
From The DNP-NMR Blog:
Homonuclear decoupling for spectral simplification of carbon-13 enriched molecules in solution-state NMR enhanced by dissolution DNP
Chinthalapalli, S., et al., Homonuclear decoupling for spectral simplification of carbon-13 enriched molecules in solution-state NMR enhanced by dissolution DNP. Phys Chem Chem Phys, 2016. 18(16): p. 11480-7.
http://www.ncbi.nlm.nih.gov/pubmed/27058951
nmrlearner
News from NMR blogs
0
06-13-2016 06:08 PM
[NMR paper] Solid-state 31P NMR investigation on the status of guanine nucleotides in paclitaxel-stabilized microtubules.
Solid-state 31P NMR investigation on the status of guanine nucleotides in paclitaxel-stabilized microtubules.
http://www.bionmr.com//www.ncbi.nlm.nih.gov/corehtml/query/egifs/http:--media.wiley.com-assets-7315-19-Wiley_FullText_120x30_orange.png Related Articles Solid-state 31P NMR investigation on the status of guanine nucleotides in paclitaxel-stabilized microtubules.
Magn Reson Chem. 2015 May;53(5):330-6
Authors: Lee GH, Oh SY, Yeo KJ, Ferdous T, Cho M, Paik Y
Abstract
Microtubule dynamics is a target for many chemotherapeutic...
nmrlearner
Journal club
0
01-09-2016 04:06 PM
[NMR paper] r TPPM: Towards improving solid-state NMR two-pulse phase-modulation heteronuclear dipolar decoupling sequence by refocusing.
r TPPM: Towards improving solid-state NMR two-pulse phase-modulation heteronuclear dipolar decoupling sequence by refocusing.
Related Articles r TPPM: Towards improving solid-state NMR two-pulse phase-modulation heteronuclear dipolar decoupling sequence by refocusing.
J Magn Reson. 2014 Apr 24;244C:68-73
Authors: Equbal A, Paul S, Mithu VS, Vinther JM, Nielsen NC, Madhu PK
Abstract
We present here a simple refocused modification, r TPPM, of the Two-Pulse Phase-Modulation (TPPM) heteronuclear decoupling method, which improves...
[NMR paper] Long-Observation-Window Band-Selective Homonuclear Decoupling: Increased Sensitivity and Resolution in Solid-State NMR Spectroscopy of Proteins
Long-Observation-Window Band-Selective Homonuclear Decoupling: Increased Sensitivity and Resolution in Solid-State NMR Spectroscopy of Proteins
Publication date: Available online 13 September 2013
Source:Journal of Magnetic Resonance</br>
Author(s): Jochem O. Struppe , Chen Yang , Yachong Wang , Roy V. Hernandez , Lisa M. Shamansky , Leonard J. Mueller</br>
Sensitivity and resolution are the two fundamental obstacles to extending solid-state nuclear magnetic resonance to even larger protein systems. Here, a novel long-observation-window band-selective...
nmrlearner
Journal club
0
09-13-2013 12:05 PM
[NMR paper] Refocused continuous-wave decoupling: a new approach to heteronuclear dipolar decoupling in solid-state NMR spectroscopy.
Refocused continuous-wave decoupling: a new approach to heteronuclear dipolar decoupling in solid-state NMR spectroscopy.
http://www.bionmr.com//www.ncbi.nlm.nih.gov/corehtml/query/egifs/http:--link.aip.org-jhtml-linkto.gif Related Articles Refocused continuous-wave decoupling: a new approach to heteronuclear dipolar decoupling in solid-state NMR spectroscopy.
J Chem Phys. 2012 Dec 7;137(21):214202
Authors: Vinther JM, Nielsen AB, Bjerring M, van Eck ER, Kentgens AP, Khaneja N, Nielsen NC
Abstract
A novel strategy for heteronuclear dipolar...
nmrlearner
Journal club
0
06-01-2013 02:03 PM
[NMR paper] Designing Dipolar Recoupling and Decoupling Experiments for Biological Solid-State NMR Using Interleaved Continuous Wave and rf Pulse Irradiation.
Designing Dipolar Recoupling and Decoupling Experiments for Biological Solid-State NMR Using Interleaved Continuous Wave and rf Pulse Irradiation.
Designing Dipolar Recoupling and Decoupling Experiments for Biological Solid-State NMR Using Interleaved Continuous Wave and rf Pulse Irradiation.
Acc Chem Res. 2013 Apr 4;
Authors: Bjerring M, Jain S, Paaske B, Vinther JM, Nielsen NC
Abstract
Rapid developments in solid-state NMR methodologyhave boosted this technique into a highly versatile tool for structural biology. The invention of...
nmrlearner
Journal club
0
04-06-2013 11:18 AM
Recoupling of native homonuclear dipolar couplings in magic-angle-spinning solid-stat
Recoupling of native homonuclear dipolar couplings in magic-angle-spinning solid-state NMR by the double-oscillating field technique.
Related Articles Recoupling of native homonuclear dipolar couplings in magic-angle-spinning solid-state NMR by the double-oscillating field technique.
J Chem Phys. 2010 Aug 14;133(6):064501
Authors: Straaso LA, Nielsen NC
A new solid-state NMR method, the double-oscillating field technique (DUO), that under magic-angle-spinning conditions produces an effective Hamiltonian proportional to the native high-field...
Five Decades of Homonuclear Dipolar Decoupling in Solid-State NMR: Status and Outlook
Linear Mode
