Solid-state NMR with magic-angle spinning (MAS) is an important method in structural biology. While NMR can provide invaluable information about local geometry on an atomic scale even for large biomolecular assemblies lacking long-range order, it is often limited by low sensitivity due to small nuclear spin polarization in thermal equilibrium. Dynamic nuclear polarization (DNP) has evolved during the last decades to become a powerful method capable of increasing this sensitivity by two to three...
Endogenous Dynamic Nuclear Polarization for Sensitivity Enhancement in Solid-State NMR of Electrode Materials #DNPNMR
From The DNP-NMR Blog:
Endogenous Dynamic Nuclear Polarization for Sensitivity Enhancement in Solid-State NMR of Electrode Materials #DNPNMR
Harchol, Adi, Guy Reuveni, Vitalii Ri, Brijith Thomas, Raanan Carmieli, Rolfe H. Herber, Chunjoong Kim, and Michal Leskes. “Endogenous Dynamic Nuclear Polarization for Sensitivity Enhancement in Solid-State NMR of Electrode Materials.” The Journal of Physical Chemistry C 124, no. 13 (April 2, 2020): 7082–90.
https://doi.org/10.1021/acs.jpcc.0c00858.
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05-16-2020 02:10 AM
[NMR paper] Biomolecular complex viewed by dynamic nuclear polarization solid-state NMR spectroscopy.
Biomolecular complex viewed by dynamic nuclear polarization solid-state NMR spectroscopy.
Related Articles Biomolecular complex viewed by dynamic nuclear polarization solid-state NMR spectroscopy.
Biochem Soc Trans. 2020 May 07;:
Authors: Chakraborty A, Deligey F, Quach J, Mentink-Vigier F, Wang P, Wang T
Abstract
Solid-state nuclear magnetic resonance (ssNMR) is an indispensable tool for elucidating the structure and dynamics of insoluble and non-crystalline biomolecules. The recent advances in the sensitivity-enhancing...
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05-08-2020 06:11 PM
Dynamic nuclear polarization for sensitivity enhancement in modern solid-state NMR #DNPNMR
From The DNP-NMR Blog:
Dynamic nuclear polarization for sensitivity enhancement in modern solid-state NMR #DNPNMR
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Lilly Thankamony, A.S., et al., Dynamic nuclear polarization for sensitivity enhancement in modern solid-state NMR. Prog Nucl Magn Reson Spectrosc, 2017. 102-103(Supplement C): p. 120-195.
https://www.ncbi.nlm.nih.gov/pubmed/29157490
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11-30-2017 01:10 AM
Dynamic nuclear polarization for sensitivity enhancement in modern solid-state NMR
Dynamic nuclear polarization for sensitivity enhancement in modern solid-state NMR
Publication date: Available online 23 July 2017
Source:Progress in Nuclear Magnetic Resonance Spectroscopy</br>
Author(s): Aany Sofia Lilly Thankamony, Johannes J. Wittmann, Monu Kaushik, Björn Corzilius</br>
The field of dynamic nuclear polarization has undergone tremendous developments and diversification since its inception more than 6 decades ago. In this review we will provide an in-depth overview of the relevant topics involved in DNP-enhanced MAS NMR spectroscopy. This...
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07-24-2017 10:10 AM
Up to 100% Improvement in Dynamic Nuclear Polarization Solid-State NMR Sensitivity Enhancement of Polymers by Removing Oxygen
From The DNP-NMR Blog:
Up to 100% Improvement in Dynamic Nuclear Polarization Solid-State NMR Sensitivity Enhancement of Polymers by Removing Oxygen
Le, D., et al., Up to 100% Improvement in Dynamic Nuclear Polarization Solid-State NMR Sensitivity Enhancement of Polymers by Removing Oxygen. Macromol Rapid Commun, 2015: p. n/a-n/a.
http://www.ncbi.nlm.nih.gov/pubmed/26010134
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06-26-2015 09:55 PM
Analysis of sensitivity enhancement by dynamic nuclear polarization in solid-state NMR: a case study of functionalized mesoporous materials
From The DNP-NMR Blog:
Analysis of sensitivity enhancement by dynamic nuclear polarization in solid-state NMR: a case study of functionalized mesoporous materials
Kobayashi, T., et al., Analysis of sensitivity enhancement by dynamic nuclear polarization in solid-state NMR: a case study of functionalized mesoporous materials. Phys Chem Chem Phys, 2013. 15(15): p. 5553-62.
http://www.ncbi.nlm.nih.gov/pubmed/23459985
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04-17-2013 08:15 PM
Analysis of sensitivity enhancement by dynamic nuclear polarization in solid-state NMR: a case study of functionalized mesoporous materials
From the The DNP-NMR Blog:
Analysis of sensitivity enhancement by dynamic nuclear polarization in solid-state NMR: a case study of functionalized mesoporous materials
Kobayashi, T., et al., Analysis of sensitivity enhancement by dynamic nuclear polarization in solid-state NMR: a case study of functionalized mesoporous materials. Phys Chem Chem Phys, 2013. 15(15): p. 5553-62.
http://www.ncbi.nlm.nih.gov/pubmed/23459985
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04-15-2013 08:52 AM
Straightforward, effective calibration of SPINAL-64 decoupling results in the enhancement of sensitivity and resolution of biomolecular solid-state NMR
Straightforward, effective calibration of SPINAL-64 decoupling results in the enhancement of sensitivity and resolution of biomolecular solid-state NMR
Publication year: 2010
Source: Journal of Magnetic Resonance, In Press, Accepted Manuscript, Available online 31 December 2010</br>
Gemma, Comellas , Jakob J., Lopez , Andrew J., Nieuwkoop , Luisel R., Lemkau , Chad M., Rienstra</br>
We describe a simple yet highly effective optimization strategy for SPINAL-64 1H decoupling conditions for magic-angle spinning solid-state NMR. With adjustment of the phase angles in a coupled manner,...
Dynamic Nuclear Polarization for Sensitivity Enhancement in Biomolecular Solid-State NMR
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