In the last three decades, the scope of solid-state NMR has expanded to exploring complex biomolecules, from large protein assemblies to intact cells at atomic-level resolution. This diversity in macromolecules frequently features highly flexible components whose insoluble environment precludes the use of solution NMR to study their structure and interactions. While High-resolution Magic-Angle Spinning (HR-MAS) probes offer the capacity for gradient-based ąH-detected spectroscopy in solids, such...
Carbon-carbon spin-spin coupling constants: Practical applications of theoretical calculations
Carbon-carbon spin-spin coupling constants: Practical applications of theoretical calculations
Publication date: April 2018
Source:Progress in Nuclear Magnetic Resonance Spectroscopy, Volume 105</br>
Author(s): Leonid B. Krivdin</br>
Practical applications of theoretical calculations of carbon-carbon spin-spin coupling constants in particular classes of organic and bioorganic molecules are reviewed, concentrating mainly on saturated, unsaturated, aromatic and heteroaromatic compounds and their functional derivatives as well as on carbohydrates and natural...
nmrlearner
Journal club
0
04-14-2018 01:49 PM
[NMR paper] Determining rotational dynamics of the guanidino group of arginine side chains in proteins by carbon-detected NMR.
Determining rotational dynamics of the guanidino group of arginine side chains in proteins by carbon-detected NMR.
Related Articles Determining rotational dynamics of the guanidino group of arginine side chains in proteins by carbon-detected NMR.
Chem Commun (Camb). 2017 Aug 25;:
Authors: Gerecht K, Figueiredo AM, Hansen DF
Abstract
Arginine residues are imperative for many active sites and protein-interaction interfaces. A new NMR-based method is presented to determine the rotational dynamics around the N?-C? bond of...
Free-Standing Mesoporous Carbon Thin Films with Highly Ordered Pore Architectures for Nanodevices
Free-Standing Mesoporous Carbon Thin Films with Highly Ordered Pore Architectures for Nanodevices
Dan Feng, Yingying Lv, Zhangxiong Wu, Yuqian Dou, Lu Han, Zhenkun Sun, Yongyao Xia, Gengfeng Zheng and Dongyuan Zhao
http://pubs.acs.org/appl/literatum/publisher/achs/journals/content/jacsat/0/jacsat.ahead-of-print/ja2056227/aop/images/medium/ja-2011-056227_0008.gif
Journal of the American Chemical Society
DOI: 10.1021/ja2056227
http://feeds.feedburner.com/~ff/acs/jacsat?d=yIl2AUoC8zA
http://feeds.feedburner.com/~r/acs/jacsat/~4/kH5IriZSWVA