[ASAP] Revealing the Surface Structure of CdSe Nanocrystals by Dynamic Nuclear Polarization-Enhanced 77Se and 113Cd Solid-State NMR Spectroscopy
Revealing the Surface Structure of CdSe Nanocrystals by Dynamic Nuclear Polarization-Enhanced 77Se and 113Cd Solid-State NMR Spectroscopy
Yunhua Chen, Rick W. Dorn, Michael P. Hanrahan, Lin Wei, Rafael Blome-Ferna?ndez, Alan M. Medina-Gonzalez, Marquix A. S. Adamson, Anne H. Flintgruber, Javier Vela, and Aaron J. Rossini
https://pubs.acs.org/na101/home/literatum/publisher/achs/journals/content/jacsat/0/jacsat.ahead-of-print/jacs.1c03162/20210604/images/medium/ja1c03162_0007.gif
Journal of the American Chemical Society
DOI: 10.1021/jacs.1c03162...
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06-05-2021 09:30 AM
Sensitivity-Enhanced 207 Pb Solid-State NMR Spectroscopy for the Rapid, Non-Destructive Characterization of Organolead Halide Perovskites #DNPNMR
From The DNP-NMR Blog:
Sensitivity-Enhanced 207 Pb Solid-State NMR Spectroscopy for the Rapid, Non-Destructive Characterization of Organolead Halide Perovskites #DNPNMR
Hanrahan, Michael P., Long Men, Bryan A. Rosales, Javier Vela, and Aaron J. Rossini. “Sensitivity-Enhanced 207 Pb Solid-State NMR Spectroscopy for the Rapid, Non-Destructive Characterization of Organolead Halide Perovskites.” Chemistry of Materials, October 4, 2018.
https://doi.org/10.1021/acs.chemmater.8b01899.
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11-25-2018 06:02 AM
Optimization of an absolute sensitivity in a glassy matrix during DNP-enhanced multidimensional solid-state NMR experiments
From The DNP-NMR Blog:
Optimization of an absolute sensitivity in a glassy matrix during DNP-enhanced multidimensional solid-state NMR experiments
Takahashi, H., et al., Optimization of an absolute sensitivity in a glassy matrix during DNP-enhanced multidimensional solid-state NMR experiments. J Magn Reson, 2013. 239C(0): p. 91-99.
http://www.ncbi.nlm.nih.gov/pubmed/24480716
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02-10-2014 08:46 PM
[NMR paper] The Fantastic Four: A plug 'n' play set of optimal control pulses for enhancing NMR spectroscopy.
From Mendeley Biomolecular NMR group:
The Fantastic Four: A plug 'n' play set of optimal control pulses for enhancing NMR spectroscopy.
Journal of magnetic resonance (San Diego, Calif. : 1997) (2013). Pages: 16-31. Manoj Nimbalkar, Burkhard Luy, Thomas E Skinner, Jorge L Neves, Naum I Gershenzon, Kyryl Kobzar, Wolfgang Bermel, Steffen J Glaser et al.
We present highly robust, optimal control-based shaped pulses designed to replace all 90° and 180° hard pulses in a given pulse sequence for improved performance. Special attention was devoted to ensuring that the pulses can be simply...
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10-17-2013 12:49 PM
[NMR paper] The Fantastic Four: A plug 'n' play set of optimal control pulses for enhancing NMR spectroscopy.
From Mendeley Biomolecular NMR group:
The Fantastic Four: A plug 'n' play set of optimal control pulses for enhancing NMR spectroscopy.
Journal of magnetic resonance (San Diego, Calif. : 1997) (2013). Pages: 16-31. Manoj Nimbalkar, Burkhard Luy, Thomas E Skinner, Jorge L Neves, Naum I Gershenzon, Kyryl Kobzar, Wolfgang Bermel, Steffen J Glaser et al.
We present highly robust, optimal control-based shaped pulses designed to replace all 90° and 180° hard pulses in a given pulse sequence for improved performance. Special attention was devoted to ensuring that the pulses can be simply...
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04-11-2013 03:08 PM
[NMR paper] Sensitivity enhancement in two-dimensional solid-state NMR spectroscopy by transverse
Sensitivity enhancement in two-dimensional solid-state NMR spectroscopy by transverse mixing.
Related Articles Sensitivity enhancement in two-dimensional solid-state NMR spectroscopy by transverse mixing.
Chemphyschem. 2004 Jun 21;5(6):863-8
Authors: Tycko R
The sensitivity of two-dimensional (2D) 13C-13C solid-state NMR spectroscopy under magic-angle spinning (MAS) is shown to be enhanced by the use of transverse polarization transfer in place of the conventional longitudinal polarization transfer. Experimental results are reported for 2D...
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11-24-2010 09:51 PM
[NMR paper] Transverse dephasing optimized solid-state NMR spectroscopy.
Transverse dephasing optimized solid-state NMR spectroscopy.
Related Articles Transverse dephasing optimized solid-state NMR spectroscopy.
J Am Chem Soc. 2003 Nov 19;125(46):13938-9
Authors: De Paëpe G, Giraud N, Lesage A, Hodgkinson P, Böckmann A, Emsley L
It is shown how coherence lifetimes in solid-state NMR experiments can be controlled. New decoupling schemes are introduced which actively optimize dephasing times, providing increases of up to a factor of 2 with respect to the best existing schemes. The new schemes are implemented in...