The 13C background signal can be distinguished from resonances of 13C-enriched xenobiotics by the absence of a 12C component, detected by combined analysis of 13C-filtered and -edited proton NMR spectra.
Journal Highlight: Determination of free fatty acids in edible oils by 1H NMR spectroscopy
Journal Highlight: Determination of free fatty acids in edible oils by 1H NMR spectroscopy
http://www.spectroscopynow.com/common/images/thumbnails/13c10b7ddda.jpgA novel proton NMR assay for the determination of free fatty acids in edible oils is a suitable alternative to the acid value method.
Source: Spectroscopynow.com
[Question from NMRWiki Q&A forum] 2D NOESY filtered/edited experiments
2D NOESY filtered/edited experiments
what are the name for 2D NOESY filtered/edited experiments like F1fF2f, F1fF2e, F2f, F1eF2e in Bruker 700MHz ?.Here is the link of that paper which has above experimentshttp://www.ncbi.nlm.nih.gov/pubmed/14739639
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The use of 1Hâ??31P GHMBC and covariance NMR to unambiguously determine phosphate ester linkages in complex polysaccharide mixtures
The use of 1Hâ??31P GHMBC and covariance NMR to unambiguously determine phosphate ester linkages in complex polysaccharide mixtures
Abstract Poly- and oligo-saccharides are commonly employed as antigens in many vaccines. These antigens contain phosphoester structural elements that are crucial to the antigenicity, and hence the effectiveness of the vaccine. Nuclear Magnetic Resonance (NMR) is a powerful tool for the site-specific identification of phosphoesters in saccharides. We describe here two advances in the characterization of phosphoesters in saccharides: (1) the use of 1Hâ??31P...
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09-19-2011 04:45 AM
Analysis of complex mixtures using high-resolution nuclear magnetic resonance spectroscopy and chemometrics
Analysis of complex mixtures using high-resolution nuclear magnetic resonance spectroscopy and chemometrics
Publication year: 2011
Source: Progress in Nuclear Magnetic Resonance Spectroscopy, In Press, Accepted Manuscript, Available online 12 May 2011</br>
James S., McKenzie , James A., Donarski , Julie C., Wilson , Adrian J., Charlton</br>
*Highlights:*? Analysis of complex mixtures using NMR spectroscopy. ? Use of chemometrics for interpretation of spectra. ? Review of sample handling approaches. ? Discussion of spectral processing methods. ? Discussion of supervised and...
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05-13-2011 07:41 AM
[NMR paper] NMR spectroscopic filtration of polypeptides and proteins in complex mixtures.
NMR spectroscopic filtration of polypeptides and proteins in complex mixtures.
Related Articles NMR spectroscopic filtration of polypeptides and proteins in complex mixtures.
J Biomol NMR. 2004 Aug;29(4):505-16
Authors: Rajagopalan S, Chow C, Raghunathan V, Fry CG, Cavagnero S
Due to the inherent complexity of the natural biological environment, most studies on polypeptides, proteins and nucleic acids have so far been performed in vitro, away from physiologically relevant conditions. Nuclear magnetic resonance is an ideal technique to extend...