The text Organic Structures from 2D NMR Spectra contains a graded set of structural problems employing 2D-NMR spectroscopy. The Instructors Guide and Solutions Manual to Organic Structures from 2D NMR Spectra is a set of step-by-step worked solutions to every problem in Organic Structures from 2D NMR Spectra. While it is absolutely clear that there are many ways to get to the correct solution of any of the problems, the instructors guide contains at least one complete pathway to every one of the questions....
Organic Structures from 2D NMR Spectra
Organic Structures from 2D NMR Spectra
http://media.wiley.com/product_data/coverImage/43/11188689/1118868943.jpgThe derivation of structural information from spectroscopic data is now an integral part of organic chemistry courses at all Universities. Over recent years, a number of powerful two-dimensional NMR techniques (e.g. HSQC, HMBC, TOCSY, COSY and NOESY) have been developed and these have vastly expanded the amount of structural information that can be obtained by NMR spectroscopy. Improvements in NMR instrumentation now mean that 2D NMR spectra are routinely (and sometimes...
[U. of Ottawa NMR Facility Blog] Manual Phase Correction of 1D Spectra - Video Tutorial
Manual Phase Correction of 1D Spectra - Video Tutorial
In some cases where there are baseline issues, automatic phase correction may not do a satisfactory job. It then becomes necessary to correct the phase manually. The following video demonstrates how to manually phase correct a 1D NMR spectrum in TOPSPIN.
http://1.bp.blogspot.com/-ILGz-b6mky0/Ubod-foqmQI/AAAAAAAABLU/FZmS3vhDv38/s400/1d_phasing.jpg
http://feeds.feedburner.com/~ff/UniversityOfOttawaNmrFacilityBlog?d=yIl2AUoC8zA
http://feeds.feedburner.com/~r/UniversityOfOttawaNmrFacilityBlog/~4/Xu9yQ1y7ZNo
Source: University...
nmrlearner
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06-14-2013 07:04 AM
Organic Structures from Spectra, 5th Edition
Organic Structures from Spectra, 5th Edition
http://media.wiley.com/product_data/coverImage/94/11183254/1118325494.jpgThe derivation of structural information from spectroscopic data is now an integral part of organic chemistry courses at all Universities. A critical part of any such course is a suitable set of problems to develop the student’s understanding of how structures are determined from spectra. Organic Structures from Spectra, Fifth Edition is a carefully chosen set of more than 280 structural problems employing the major modern spectroscopic techniques, a selection of 27...
nmrlearner
Books
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04-20-2013 02:07 AM
Protein NMR - A Practical Guide - Solution NMR Spectra
Below is a Google-cached version of Protein NMR - A Practical Guide - Solution NMR Spectra page from www.protein-nmr.org.uk crashed on 11/6/11. You may want to check first if the site has been restored.
Spectrum Descriptions
This page contains a list of the solution NMR experiments most commonly used in protein NMR assignment and structure calculation. For each experiment there is an illustration showing which atoms are observed (pink) and through which atoms magnetisation flows (light blue). An example spectrum shows what it should look like and particular features and...
markber
Cashed version of protein-nmr.org.uk
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11-06-2011 08:45 PM
[NMR paper] Sources of and solutions to problems in the refinement of protein NMR structures agai
Sources of and solutions to problems in the refinement of protein NMR structures against torsion angle potentials of mean force.
Related Articles Sources of and solutions to problems in the refinement of protein NMR structures against torsion angle potentials of mean force.
J Magn Reson. 2000 Oct;146(2):249-54
Authors: Kuszewski J, Clore GM
It is often the case that a substantial number of torsion angles (both backbone and sidechain) in structures of proteins and nucleic acids determined by NMR are found in physically unlikely and...